{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,10,12]],"date-time":"2025-10-12T04:42:03Z","timestamp":1760244123223,"version":"build-2065373602"},"reference-count":16,"publisher":"MDPI AG","issue":"8","license":[{"start":{"date-parts":[[2005,8,31]],"date-time":"2005-08-31T00:00:00Z","timestamp":1125446400000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/3.0\/"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Molecules"],"abstract":"<jats:p>In this paper we elected to nitrate p-xylene because this compound has onlyone mononitro- and trinitro- isomer. Trinitro-p-xylene was used as a starting material forthe synthesis of other compounds in subsequent work. The mononitration of p-xylene canbe easily carried out at 30\u00b0C. Nitro-p-xylene is easily nitrated to dinitro-p-xylene at atemperature of 80\u00b0C. The trinitro-p-xylene can be obtained at 120\u00b0C. Single crystals of2,3-dinitro-p-xylene and 2,3,5-trinitro-p-xylene were grown using theslow cooling method and we report the X-ray structure of the former. The thermaldecomposition of the compounds was studied using differential scanning calorimetry(DSC) and thermogravimetry-derivative thermogravimetry (TG-DTG) techniques andFT-IR. The target compounds were also characterized by 1H-NMR, 13C-NMR and MS.<\/jats:p>","DOI":"10.3390\/10080978","type":"journal-article","created":{"date-parts":[[2008,10,25]],"date-time":"2008-10-25T13:32:11Z","timestamp":1224941531000},"page":"978-989","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":5,"title":["Synthesis and Characterization of Nitro-p-xylenes"],"prefix":"10.3390","volume":"10","author":[{"given":"L.","family":"Yan-Hong","sequence":"first","affiliation":[{"name":"State Key Laboratory of Prevention and Control of Explosion, Beijing Institute of Technology, P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Z.","family":"Tong-Lai","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Prevention and Control of Explosion, Beijing Institute of Technology, P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Z.","family":"Jian-Guo","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Prevention and Control of Explosion, Beijing Institute of Technology, P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"G.","family":"Jin-Yu","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Prevention and Control of Explosion, Beijing Institute of Technology, P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Y.","family":"Kai-Bei","sequence":"additional","affiliation":[{"name":"Center of Analysis and Test of Chengdu Branch, Chinese Academy of Sciences, P.R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"1968","published-online":{"date-parts":[[2005,8,31]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","unstructured":"Guisnet, M., Gnep, N. S., and Morin, S. (2000). Micropor. Mesopor. 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