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In this study, an acidified acetonitrile-based QuEChERS method was developed and validated for the multiresidue determination of 136 pesticides in Tahiti lime (Citrus latifolia) using ultra-high-performance liquid chromatography coupled with tandem mass spectrometry (UHPLC\u2013MS\/MS). The proposed approach employs 1% formic acid in acetonitrile and omits the conventional clean-up step, aiming to improve analyte recovery and analytical throughput. Method validation was performed according to SANTE guidelines, demonstrating satisfactory linearity (R2 \u2265 0.99 for all analytes), limits of quantification of 0.01 mg kg\u22121, and recoveries within 70\u2013120%, with relative standard deviations \u2264 20% for the vast majority of compounds. Notably, the method achieved consistent and reliable performance for 12 acidic pesticides, which are typically problematic in conventional QuEChERS approaches. Application to 22 real samples revealed the presence of 14 pesticide residues, with some compounds exceeding European Union (EU) maximum residue limits. The proposed method provides a simple, efficient, and robust alternative for comprehensive pesticide monitoring in citrus fruits, with particular advantages for the determination of acidic compounds in highly complex matrices.<\/jats:p>","DOI":"10.3390\/foods15172967","type":"journal-article","created":{"date-parts":[[2026,8,24]],"date-time":"2026-08-24T11:47:19Z","timestamp":1787572039000},"page":"2967","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Acidified Acetonitrile Extraction and Ultra-High Performance Liquid Chromatography\u2013Tandem Mass Spectrometry for Multiresidue Determination of 136 Pesticides in Tahiti Lime (Citrus latifolia)"],"prefix":"10.3390","volume":"15","author":[{"ORCID":"https:\/\/orcid.org\/0000-0003-0171-5393","authenticated-orcid":false,"given":"Karolaine da Silva","family":"Albarnaz","sequence":"first","affiliation":[{"name":"Laboratory of Pesticide Residue Analysis (LARP), Department of Chemistry, Federal University of Santa Maria, Av. Roraima, 1000, Santa Maria 97105-900, RS, Brazil"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Juliana Diniz de Barros","family":"Kuntz","sequence":"additional","affiliation":[{"name":"Laboratory of Pesticide Residue Analysis (LARP), Department of Chemistry, Federal University of Santa Maria, Av. Roraima, 1000, Santa Maria 97105-900, RS, Brazil"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Luana","family":"Floriano","sequence":"additional","affiliation":[{"name":"Laboratory of Pesticide Residue Analysis (LARP), Department of Chemistry, Federal University of Santa Maria, Av. Roraima, 1000, Santa Maria 97105-900, RS, Brazil"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Franciele F\u00e1tima","family":"Machado","sequence":"additional","affiliation":[{"name":"Laboratory of Pesticide Residue Analysis (LARP), Department of Chemistry, Federal University of Santa Maria, Av. Roraima, 1000, Santa Maria 97105-900, RS, Brazil"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1328-1860","authenticated-orcid":false,"given":"Martha Bohrer","family":"Adaime","sequence":"additional","affiliation":[{"name":"Laboratory of Pesticide Residue Analysis (LARP), Department of Chemistry, Federal University of Santa Maria, Av. Roraima, 1000, Santa Maria 97105-900, RS, Brazil"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5971-1785","authenticated-orcid":false,"given":"Renato","family":"Zanella","sequence":"additional","affiliation":[{"name":"Laboratory of Pesticide Residue Analysis (LARP), Department of Chemistry, Federal University of Santa Maria, Av. Roraima, 1000, Santa Maria 97105-900, RS, Brazil"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6012-7172","authenticated-orcid":false,"given":"Osmar Damian","family":"Prestes","sequence":"additional","affiliation":[{"name":"Laboratory of Pesticide Residue Analysis (LARP), Department of Chemistry, Federal University of Santa Maria, Av. Roraima, 1000, Santa Maria 97105-900, RS, Brazil"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1968","published-online":{"date-parts":[[2026,8,24]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","unstructured":"Popkova, E.G., Bogoviz, A.V., Sergi, B.S., Kaurova, O.V., and Maloletko, A.N. (2024). Changing the Global Production and Trade of Citrus Fruits. Sustainable Development of the Agrarian Economy Based on Digital Technologies and Smart Innovations, Springer. Advances in Science, Technology & Innovation.","DOI":"10.1007\/978-3-031-51272-8"},{"key":"ref_2","doi-asserted-by":"crossref","unstructured":"Pereira Gonzatto, M., and Scherer Santos, J. (2023). Introductory Chapter: World Citrus Production and Research. Citrus Research\u2014Horticultural and Human Health Aspects, IntechOpen.","DOI":"10.5772\/intechopen.110519"},{"key":"ref_3","doi-asserted-by":"crossref","unstructured":"Chand, G., Akhtar, M.N., and Kumar, S. (2020). Diseases of Fruits and Vegetable Crops: Recent Management Approaches, Apple Academic Press. [1st ed.].","DOI":"10.1201\/9780429322181"},{"key":"ref_4","doi-asserted-by":"crossref","first-page":"123","DOI":"10.1007\/s44279-024-00141-z","article-title":"The implications of pesticide residue in food crops on human health: A critical review","volume":"2","author":"Beyuo","year":"2024","journal-title":"Discov. Agric."},{"key":"ref_5","unstructured":"European Commission (2009). EU Pesticides Database, European Commission. Available online: https:\/\/food.ec.europa.eu\/plants\/pesticides\/eu-pesticides-database_en."},{"key":"ref_6","unstructured":"Ag\u00eancia Nacional de Vigil\u00e2ncia Sanit\u00e1ria (ANVISA) (2026, May 21). Monografias de Agrot\u00f3xicos, Available online: https:\/\/www.gov.br\/anvisa\/pt-br\/acessoainformacao\/dadosabertos\/informacoes-analiticas\/monografias-de-agrotoxicos."},{"key":"ref_7","doi-asserted-by":"crossref","first-page":"127381","DOI":"10.1016\/j.chemosphere.2020.127381","article-title":"Occurrence, temporal variation, quality and safety assessment of pesticide residues on citrus fruits in China","volume":"258","author":"Li","year":"2020","journal-title":"Chemosphere"},{"key":"ref_8","doi-asserted-by":"crossref","first-page":"50012","DOI":"10.1007\/s11356-024-34525-x","article-title":"Advances on multiclass pesticide residue determination in citrus fruits and citrus-derived products\u2014A critical review","volume":"31","author":"Antonio","year":"2024","journal-title":"Environ. Sci. Pollut. Res."},{"key":"ref_9","doi-asserted-by":"crossref","first-page":"753","DOI":"10.1016\/j.fshw.2022.03.001","article-title":"Dietary bioactives and essential oils of lemon and lime fruits","volume":"11","author":"Liu","year":"2022","journal-title":"Food Sci. Hum. Wellness"},{"key":"ref_10","doi-asserted-by":"crossref","first-page":"e994","DOI":"10.1590\/3085-89092025994","article-title":"Performance of \u2018Tahiti\u2019 Acid Lime Grafted onto Rootstocks in North of Mato Grosso","volume":"1","author":"Roncatto","year":"2025","journal-title":"Fruit Crop Sci. J."},{"key":"ref_11","doi-asserted-by":"crossref","first-page":"4819","DOI":"10.1021\/acs.jafc.7b00243","article-title":"Matrix effects and interferences of different citrus fruit coextractives in pesticide residue analysis using ultrahigh-performance liquid chromatography\u2013high-resolution mass spectrometry","volume":"65","author":"Besil","year":"2017","journal-title":"J. Agric. Food Chem."},{"key":"ref_12","doi-asserted-by":"crossref","first-page":"519","DOI":"10.1016\/j.chemosphere.2018.05.116","article-title":"Simultaneous analysis of 310 pesticide multiresidues using UHPLC-MS\/MS in brown rice, orange, and spinach","volume":"207","author":"Lee","year":"2018","journal-title":"Chemosphere"},{"key":"ref_13","doi-asserted-by":"crossref","first-page":"412","DOI":"10.1093\/jaoac\/86.2.412","article-title":"Fast and easy multiresidue method employing acetonitrile extraction\/partitioning and \u201cdispersive solid-phase extraction\u201d for the determination of pesticide residues in produce","volume":"86","author":"Anastassiades","year":"2003","journal-title":"J. AOAC Int."},{"key":"ref_14","unstructured":"AOAC International (2007). AOAC Official Method 2007.01: Pesticide Residues in Foods by Acetonitrile Extraction and Partitioning with Magnesium Sulfate Gas Chromatography\/Mass Spectrometry and Liquid Chromatography\/Tandem Mass Spectrometry, AOAC International. First Action 2007."},{"key":"ref_15","unstructured":"European Committee for Standardization (CEN) (2007). Foods of Plant Origin\u2014Determination of Pesticide Residues Using GC-MS and\/or LC-MS\/MS Following Acetonitrile Extraction\/Partitioning and Clean-up by Dispersive SPE (QuEChERS-Method), CEN. prEN 15662 Version 2007-10-24."},{"key":"ref_16","doi-asserted-by":"crossref","unstructured":"Yuan, X., Kim, C.J., Lee, R., Kim, M., Shin, H.J., Kim, L., Jeong, W.T., Shin, Y., Kyung, K.S., and Noh, H.H. (2022). Validation of a Multi-Residue Analysis Method for 287 Pesticides in Citrus Fruits Mandarin Orange and Grapefruit Using Liquid Chromatography\u2013Tandem Mass Spectrometry. Foods, 11.","DOI":"10.3390\/foods11213522"},{"key":"ref_17","doi-asserted-by":"crossref","first-page":"4061","DOI":"10.1080\/03067319.2021.1921761","article-title":"Optimization and Evaluation of Four Multi-Residue Methods for the Determination of Pesticide Residues in Orange Oil Using LC-MS\/MS and GC-MS\/MS: A Comparative Study","volume":"103","author":"Elshabrawy","year":"2023","journal-title":"Int. J. Environ. Anal. Chem."},{"key":"ref_18","doi-asserted-by":"crossref","first-page":"5107","DOI":"10.1021\/jf505539e","article-title":"Development of an Automated Column Solid-Phase Extraction Cleanup of QuEChERS Extracts, Using a Zirconia-Based Sorbent, for Pesticide Residue Analyses by LC-MS\/MS","volume":"63","author":"Morris","year":"2015","journal-title":"J. Agric. Food Chem."},{"key":"ref_19","doi-asserted-by":"crossref","first-page":"906","DOI":"10.1016\/j.foodcont.2007.09.002","article-title":"Analysis of 140 pesticides from conventional farming foodstuff samples after extraction with the modified QuEChERS method","volume":"19","author":"Lesueur","year":"2008","journal-title":"Food Control"},{"key":"ref_20","doi-asserted-by":"crossref","first-page":"130","DOI":"10.21448\/ijsm.408174","article-title":"Development and validation of modified QuEChERS method coupled with GC-MS\/MS for 123 pesticide residues in food","volume":"5","author":"Harmandar","year":"2018","journal-title":"Int. J. Sec. Metab."},{"key":"ref_21","doi-asserted-by":"crossref","first-page":"65","DOI":"10.1007\/978-1-61779-136-9_4","article-title":"QuEChERS Sample Preparation Approach for Mass Spectrometric Analysis of Pesticide Residues in Foods","volume":"Volume 747","author":"Zweigenbaum","year":"2011","journal-title":"Mass Spectrometry in Food Safety"},{"key":"ref_22","doi-asserted-by":"crossref","first-page":"3525","DOI":"10.1002\/jssc.201500625","article-title":"Comparison of extraction solvents and sorbents in the quick, easy, cheap, effective, rugged, and safe method for the determination of pesticide multiresidue in fruits by ultra-high-performance liquid chromatography with tandem mass spectrometry","volume":"38","author":"Liu","year":"2015","journal-title":"J. Sep. Sci."},{"key":"ref_23","doi-asserted-by":"crossref","first-page":"100223","DOI":"10.1016\/j.greeac.2025.100223","article-title":"Determination of neonicotinoids and other residues in orange pollen by micro-QuEChERS and UHPLC\u2013MS\/MS","volume":"12","author":"Almeida","year":"2025","journal-title":"Green Anal. Chem."},{"key":"ref_24","doi-asserted-by":"crossref","first-page":"1511","DOI":"10.1007\/s12161-020-01921-1","article-title":"Dilution of QuEChERS Extracts Without Cleanup Improves Results in the UHPLC-MS\/MS Multiresidue Analysis of Pesticides in Tomato","volume":"14","author":"Stringhini","year":"2021","journal-title":"Food Anal. Methods"},{"key":"ref_25","doi-asserted-by":"crossref","unstructured":"Jeong, M.-J., Kim, S.-M., Lee, Y.-J., Lee, Y.-H., Eun, H.-R., Eom, M., Jang, G.-H., Lee, J., Jo, H.-W., and Moon, J.-K. (2024). Simultaneous Analysis of 504 Pesticide Multiresidues in Crops Using UHPLC-QTOF at MS1 and MS2 Levels. Foods, 13.","DOI":"10.3390\/foods13213503"},{"key":"ref_26","unstructured":"European Commission (2026, March 21). Analytical Quality Control and Method Validation Procedures for Pesticide Residues Analysis in Food and Feed, Document No. SANTE\/11312\/2021 v2026. Available online: https:\/\/eurl-pesticides.eu\/docs\/public\/tmplt_article.asp?CntID=727."},{"key":"ref_27","unstructured":"European Commission (2026, March 25). Analysis of Acidic Pesticides and Metabolites via CEN-QuEChERS and FA-QuEChERS. European Union Reference Laboratory for Pesticide Residues: 2024. Available online: https:\/\/www.eurl-pesticides.eu\/docs\/public\/tmplt_article.asp?LabID=200&CntID=1301&Theme_ID=1&Pdf=False&Lang=EN."},{"key":"ref_28","doi-asserted-by":"crossref","first-page":"6861","DOI":"10.1007\/s00216-018-1286-1","article-title":"Analysis of Thermally Labile Pesticides by On-Column Injection Gas Chromatography in Fruit and Vegetables","volume":"410","author":"Hakme","year":"2018","journal-title":"Anal. Bioanal. Chem."},{"key":"ref_29","doi-asserted-by":"crossref","first-page":"224","DOI":"10.1080\/03067319.2019.1588263","article-title":"Determination of 10 pesticides, newly registered in Egypt, using modified QuEChERS method in combination with gas and liquid chromatography coupled with tandem mass spectrometric detection","volume":"99","author":"Soliman","year":"2019","journal-title":"Int. J. Environ. Anal. Chem."},{"key":"ref_30","doi-asserted-by":"crossref","unstructured":"Aslanta\u015f, S., Golge, O., Gonz\u00e1lez-Curbelo, M.\u00c1., and Kabak, B. (2023). Determination of 355 Pesticides in Lemon and Lemon Juice by LC-MS\/MS and GC-MS\/MS. Foods, 12.","DOI":"10.3390\/foods12091812"},{"key":"ref_31","doi-asserted-by":"crossref","first-page":"618","DOI":"10.1007\/s42452-019-0626-x","article-title":"Analytical methods for the routinely evaluation of pesticide residues in lemon fruits and by products","volume":"1","author":"Besil","year":"2019","journal-title":"SN Appl. Sci."},{"key":"ref_32","unstructured":"Instituto Brasileiro do Meio Ambiente e dos Recursos Naturais Renov\u00e1veis (IBAMA) (2026, May 21). Relat\u00f3rios de Comercializa\u00e7\u00e3o de Agrot\u00f3xicos, Available online: https:\/\/www.gov.br\/ibama\/pt-br\/assuntos\/quimicos-e-biologicos\/agrotoxicos\/relatorios-de-comercializacao-de-agrotoxicos."},{"key":"ref_33","unstructured":"Ag\u00eancia Nacional de Vigil\u00e2ncia Sanit\u00e1ria (ANVISA) (2026, May 21). D27\u20142,4-D, Available online: https:\/\/www.gov.br\/anvisa\/pt-br\/setorregulado\/regularizacao\/agrotoxicos\/monografias\/monografias-autorizadas\/d\/4285json-file-1\/view?utm_source=chatgpt.com."},{"key":"ref_34","doi-asserted-by":"crossref","first-page":"103314","DOI":"10.1016\/j.jfca.2019.103314","article-title":"Recent developments and applications of QuEChERS based techniques on food samples during pesticide analysis","volume":"84","author":"Musarurwa","year":"2019","journal-title":"J. Food Compos. Anal."},{"key":"ref_35","doi-asserted-by":"crossref","unstructured":"Kowalska, G., Pankiewicz, U., and Kowalski, R. (2022). Assessment of Pesticide Content in Apples and Selected Citrus Fruits Subjected to Simple Culinary Processing. Appl. Sci., 12.","DOI":"10.3390\/app12031417"},{"key":"ref_36","doi-asserted-by":"crossref","first-page":"65","DOI":"10.1016\/j.aca.2019.12.012","article-title":"Facile synthesis of a core-shell structured magnetic covalent organic framework for enrichment of organophosphorus pesticides in fruits","volume":"1101","author":"Lin","year":"2020","journal-title":"Anal. Chim. Acta"},{"key":"ref_37","doi-asserted-by":"crossref","first-page":"25","DOI":"10.1016\/j.foodchem.2015.09.010","article-title":"Optimization of a QuEChERS based method by means of central composite design for pesticide multiresidue determination in orange juice by UHPLC\u2013MS\/MS","volume":"196","author":"Rizzetti","year":"2016","journal-title":"Food Chem."},{"key":"ref_38","doi-asserted-by":"crossref","first-page":"86","DOI":"10.1016\/j.jfca.2015.02.007","article-title":"Determination of 115 pesticide residues in oranges by high-performance liquid chromatography\u2013triple-quadrupole mass spectrometry in combination with QuEChERS method","volume":"41","author":"Golge","year":"2015","journal-title":"J. Food Compos. Anal."},{"key":"ref_39","unstructured":"Ag\u00eancia Nacional de Vigil\u00e2ncia Sanit\u00e1ria (ANVISA) (2026, August 03). Programa de An\u00e1lise de Res\u00edduos de Agrot\u00f3xicos em Alimentos (PARA): Relat\u00f3rio 2024, Available online: https:\/\/www.gov.br\/anvisa\/pt-br\/assuntos\/agrotoxicos\/programa-de-analise-de-residuos-em-alimentos\/relatorios-do-programa."},{"key":"ref_40","unstructured":"European Commission (2026, August 03). Rapid Alert System for Food and Feed (RASFF): Public Search Portal. Available online: https:\/\/webgate.ec.europa.eu\/rasff-window\/screen\/search."}],"container-title":["Foods"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/www.mdpi.com\/2304-8158\/15\/17\/2967\/pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2026,8,26]],"date-time":"2026-08-26T04:25:23Z","timestamp":1787718323000},"score":1,"resource":{"primary":{"URL":"https:\/\/www.mdpi.com\/2304-8158\/15\/17\/2967"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2026,8,24]]},"references-count":40,"journal-issue":{"issue":"17","published-online":{"date-parts":[[2026,9]]}},"alternative-id":["foods15172967"],"URL":"https:\/\/doi.org\/10.3390\/foods15172967","relation":{},"ISSN":["2304-8158"],"issn-type":[{"value":"2304-8158","type":"electronic"}],"subject":[],"published":{"date-parts":[[2026,8,24]]}}}