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In this study, cellulose extracted from wheat straw was regenerated into biodegradable films using calcium-ion crosslinking and glycerol plasticization. A Box\u2013Behnken experimental design optimized cellulose content (0.35\u20130.5 g), calcium chloride concentration (200\u2013800 nm), and glycerol concentration (0.5\u20131.5%) to produce films with balanced mechanical and barrier properties. The optimized film was characterized for its physicochemical, mechanical, optical, antioxidant, and biodegradation properties and evaluated for fresh grape packaging. The film exhibited favorable mechanical strength of 30.82 \u00b1 4.70 MPa, controlled water vapor permeability of 0.59 \u00b1 0.06 10\u221210 gm\u22121 s\u22121 Pa\u22121, elongation at break of 4.36 \u00b1 0.35%, moderate transparency of 22.95 \u00b1 0.65% mm\u22121 at 600 nm, and ultraviolet light-blocking capability, allowing only 9.57 \u00b1 1.44% of UV-B at 300 nm, and an IC50 value of 0.33, indicating moderate antioxidant potential, with 35% biodegradation after 37 days at a soil moisture of 24%. During ambient storage, grapes packaged with the film reached 15% weight loss by 13 days, while slowing changes in total soluble solids, pH, titratable acidity, total phenolic content, and vitamin C, and delaying visible quality deterioration. Compared with the uncovered control, packaged grapes maintained acceptable quality for approximately six additional days, reaching 15 days of storage. Unlike conventional polystyrene film, which promoted excessive gas accumulation and fruit cracking, the wheat straw cellulose film provided a semipermeable barrier that balanced moisture and gas exchange. The systematic optimization of these formulations, followed by comprehensive characterization of the optimized films, demonstrates the potential of wheat straw cellulose as a functional material for developing cellulose films as sustainable, biodegradable packaging materials for extending the postharvest quality of fresh produce.<\/jats:p>","DOI":"10.3390\/foods15173111","type":"journal-article","created":{"date-parts":[[2026,9,1]],"date-time":"2026-09-01T12:41:18Z","timestamp":1788266478000},"page":"3111","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Valorization of Wheat Straw Cellulose into Biodegradable Packaging Films for Fresh Produce Preservation"],"prefix":"10.3390","volume":"15","author":[{"given":"Sharad","family":"Bhattarai","sequence":"first","affiliation":[{"name":"Department of Dairy and Food Science, South Dakota State University, Brookings, SD 57007, USA"}],"role":[{"vocabulary":"crossref","role":"author"},{"role":"methodology","vocabulary":"credit"},{"role":"investigation","vocabulary":"credit"},{"role":"visualization","vocabulary":"credit"},{"role":"validation","vocabulary":"credit"},{"role":"writing-original-draft","vocabulary":"credit"},{"role":"formal-analysis","vocabulary":"credit"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5422-0493","authenticated-orcid":false,"given":"Srinivas","family":"Janaswamy","sequence":"additional","affiliation":[{"name":"Department of Dairy and Food Science, South Dakota State University, Brookings, SD 57007, USA"}],"role":[{"vocabulary":"crossref","role":"author"},{"role":"conceptualization","vocabulary":"credit"},{"role":"resources","vocabulary":"credit"},{"role":"supervision","vocabulary":"credit"},{"role":"project-administration","vocabulary":"credit"},{"role":"writing-review-editing","vocabulary":"credit"},{"role":"funding-acquisition","vocabulary":"credit"}]}],"member":"1968","published-online":{"date-parts":[[2026,9,1]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"1977","DOI":"10.1098\/rstb.2008.0304","article-title":"Applications and Societal Benefits of Plastics","volume":"364","author":"Andrady","year":"2009","journal-title":"Philos. Trans. R. Soc. B Biol. Sci."},{"key":"ref_2","unstructured":"Sasu, D.D. (2026, June 27). Global Plastic Production|Statista. Available online: https:\/\/www.statista.com\/statistics\/282732\/global-production-of-plastics-since-1950\/."},{"key":"ref_3","doi-asserted-by":"crossref","unstructured":"Yun, X., and Dong, T. (2017). Fabrication of High-Barrier Plastics and Its Application in Food Packaging. Food Packaging, Academic Press.","DOI":"10.1016\/B978-0-12-804302-8.00005-4"},{"key":"ref_4","first-page":"2456","article-title":"The Science Behind Plastics: Understanding Their Traits and Uses","volume":"9","author":"Ramaswamy","year":"2024","journal-title":"Int. J. Nov. Res. Dev."},{"key":"ref_5","doi-asserted-by":"crossref","first-page":"576","DOI":"10.1002\/pc.22974","article-title":"Thermal and Biodegradation Properties of Poly(Lactic Acid)\/Fertilizer\/Oil Palm Fibers Blends Biocomposites","volume":"36","author":"Harmaen","year":"2015","journal-title":"Polym. Compos."},{"key":"ref_6","first-page":"853","article-title":"Assessing the Change in Environmental Impact Categories When Replacing Conventional Plastic with Bioplastic in Chosen Application Fields","volume":"70","author":"Walmsley","year":"2018","journal-title":"Chem. Eng. Trans."},{"key":"ref_7","doi-asserted-by":"crossref","first-page":"151","DOI":"10.1016\/j.psep.2024.05.113","article-title":"Impact of Bioplastics on Environment from Its Production to End-of-Life","volume":"188","author":"Islam","year":"2024","journal-title":"Process Saf. Environ. Prot."},{"key":"ref_8","doi-asserted-by":"crossref","first-page":"379","DOI":"10.1007\/s10311-021-01334-4","article-title":"Innovations in Applications and Prospects of Bioplastics and Biopolymers: A Review","volume":"20","author":"Nanda","year":"2021","journal-title":"Environ. Chem. Lett."},{"key":"ref_9","doi-asserted-by":"crossref","first-page":"114005","DOI":"10.1016\/j.lwt.2022.114005","article-title":"Improving the Hydrophobicity and Mechanical Properties of Starch Nanofibrous Films by Electrospinning and Cross-Linking for Food Packaging Applications","volume":"169","author":"Zhu","year":"2022","journal-title":"LWT\u2014Food Sci. Technol."},{"key":"ref_10","doi-asserted-by":"crossref","first-page":"147885","DOI":"10.1016\/j.ijbiomac.2025.147885","article-title":"Packaging through the Ages: A Heuristic Journey from Leaves to Plastics to Cellulosic Fibers and Smart Technologies","volume":"330","author":"Regmi","year":"2025","journal-title":"Int. J. Biol. Macromol."},{"key":"ref_11","doi-asserted-by":"crossref","first-page":"22","DOI":"10.1016\/j.foodchem.2017.12.067","article-title":"Feasibility of Biodegradable Based Packaging Used for Red Meat Storage during Shelf-Life: A Pilot Study","volume":"249","author":"Panseri","year":"2018","journal-title":"Food Chem."},{"key":"ref_12","doi-asserted-by":"crossref","first-page":"117","DOI":"10.1038\/s41578-021-00407-8","article-title":"Bioplastics for a Circular Economy","volume":"7","author":"Rosenboom","year":"2022","journal-title":"Nat. Rev. Mater."},{"key":"ref_13","doi-asserted-by":"crossref","first-page":"1681","DOI":"10.1007\/s00217-017-2878-2","article-title":"Innovations in the Food Packaging Market: Active Packaging","volume":"243","author":"Wyrwa","year":"2017","journal-title":"Eur. Food Res. Technol."},{"key":"ref_14","doi-asserted-by":"crossref","first-page":"1","DOI":"10.1016\/j.fpsl.2018.01.006","article-title":"Utilization of Mango Peel Extracts on the Biodegradable Films for Active Packaging","volume":"16","author":"Adilah","year":"2018","journal-title":"Food Packag. Shelf Life"},{"key":"ref_15","doi-asserted-by":"crossref","first-page":"9925","DOI":"10.1007\/s10570-023-05520-1","article-title":"Application of Cellulose and Cellulose Derivatives in Smart\/Intelligent Bio-Based Food Packaging","volume":"30","author":"Yekta","year":"2023","journal-title":"Cellulose"},{"key":"ref_16","doi-asserted-by":"crossref","first-page":"811","DOI":"10.1002\/pts.70065","article-title":"Cellulose-Based Packaging From Agricultural Residues: Extraction Technologies, Functional Performance, Emerging Applications and Future Prospects","volume":"39","author":"Paudel","year":"2026","journal-title":"Packag. Technol. Sci."},{"key":"ref_17","doi-asserted-by":"crossref","first-page":"99","DOI":"10.1016\/j.tplants.2013.09.009","article-title":"Cellulose Synthases: New Insights from Crystallography and Modeling","volume":"19","author":"Slabaugh","year":"2014","journal-title":"Trends Plant Sci."},{"key":"ref_18","doi-asserted-by":"crossref","first-page":"490","DOI":"10.1038\/s44222-025-00377-4","article-title":"Molecular Engineering of Cellulose and Its Applications","volume":"4","author":"Xu","year":"2026","journal-title":"Nat. Rev. Bioeng."},{"key":"ref_19","doi-asserted-by":"crossref","unstructured":"Shah, A.M., Zhang, H., Shahid, M., Ghazal, H., Shah, A.R., Niaz, M., Naz, T., Ghimire, K., Goswami, N., and Shi, W. (2025). The Vital Roles of Agricultural Crop Residues and Agro-Industrial By-Products to Support Sustainable Livestock Productivity in Subtropical Regions. Animals, 15.","DOI":"10.3390\/ani15081184"},{"key":"ref_20","doi-asserted-by":"crossref","first-page":"79","DOI":"10.1080\/17597269.2022.2118779","article-title":"Potential of Biofuels Production from Wheat Straw Biomass, Current Achievements and Perspectives: A Review","volume":"14","author":"Tatari","year":"2023","journal-title":"Biofuels"},{"key":"ref_21","doi-asserted-by":"crossref","unstructured":"Erenstein, O., Jaleta, M., Abdul Mottaleb, K., Sonder, K., Donovan, J., and Braun, H.J. (2022). Global Trends in Wheat Production, Consumption and Trade. Wheat Improvement: Food Security in a Changing Climate, Springer.","DOI":"10.1007\/978-3-030-90673-3_4"},{"key":"ref_22","doi-asserted-by":"crossref","unstructured":"Kova\u010devi\u0107, Z., Bischof, S., Biland\u017eija, N., and Kri\u010dka, T. (2024). Conversion of Waste Agricultural Biomass from Straw into Useful Bioproducts\u2014Wheat Fibers and Biofuels. Sustainability, 16.","DOI":"10.3390\/su16114739"},{"key":"ref_23","doi-asserted-by":"crossref","first-page":"106016","DOI":"10.1016\/j.fbio.2025.106016","article-title":"Biodegradable Packaging Films from the Alkali-Extracted Lignocellulosic Residue of Soyhulls Extend the Shelf Life of Strawberries","volume":"65","author":"Regmi","year":"2025","journal-title":"Food Biosci."},{"key":"ref_24","doi-asserted-by":"crossref","unstructured":"Regmi, S., Paudel, S., and Janaswamy, S. (2024). Development of Eco-Friendly Packaging Films from Soyhull Lignocellulose: Towards Valorizing Agro-Industrial Byproducts. Foods, 13.","DOI":"10.3390\/foods13244000"},{"key":"ref_25","doi-asserted-by":"crossref","first-page":"140672","DOI":"10.1016\/j.foodchem.2024.140672","article-title":"Biodegradable Films from Soyhull Cellulosic Residue with UV Protection and Antioxidant Properties Improve the Shelf-Life of Post-Harvested Raspberries","volume":"460","author":"Regmi","year":"2024","journal-title":"Food Chem."},{"key":"ref_26","doi-asserted-by":"crossref","first-page":"139749","DOI":"10.1016\/j.foodchem.2024.139749","article-title":"Corncob-Derived Biodegradable Packaging Films: A Sustainable Solution for Raspberry Post-Harvest Preservation","volume":"454","author":"Paudel","year":"2024","journal-title":"Food Chem."},{"key":"ref_27","doi-asserted-by":"crossref","unstructured":"Escamilla-Garc\u00eda, M., Garc\u00eda-Garc\u00eda, M.C., Gracida, J., Hern\u00e1ndez-Hern\u00e1ndez, H.M., Granados-Arvizu, J.\u00c1., Di Pierro, P., and Regalado-Gonz\u00e1lez, C. (2022). Properties and Biodegradability of Films Based on Cellulose and Cellulose Nanocrystals from Corn Cob in Mixture with Chitosan. Int. J. Mol. Sci., 23.","DOI":"10.3390\/ijms231810560"},{"key":"ref_28","doi-asserted-by":"crossref","unstructured":"Choque-Quispe, D., Choque-Quispe, Y., Ligarda-Samanez, C.A., Peralta-Guevara, D.E., Solano-Reynoso, A.M., Ramos-Pacheco, B.S., Taipe-Pardo, F., Mart\u00ednez-Huam\u00e1n, E.L., Aguirre Landa, J.P., and Agreda Cerna, H.W. (2022). Effect of the Addition of Corn Husk Cellulose Nanocrystals in the Development of a Novel Edible Film. Nanomaterials, 12.","DOI":"10.3390\/nano12193421"},{"key":"ref_29","doi-asserted-by":"crossref","first-page":"1633","DOI":"10.1039\/D5FB00872G","article-title":"Biodegradable Films Based on Alfalfa Cellulosic Residue and Carrageenan Blends for Sustainable Food Packaging","volume":"4","author":"Paudel","year":"2026","journal-title":"Sustain. Food Technol."},{"key":"ref_30","doi-asserted-by":"crossref","first-page":"151954","DOI":"10.1016\/j.ijbiomac.2026.151954","article-title":"Alkali-Digested Alfalfa Lignocellulose for Sustainable UV-Blocking Packaging Films","volume":"360","author":"Paudel","year":"2026","journal-title":"Int. J. Biol. Macromol."},{"key":"ref_31","doi-asserted-by":"crossref","first-page":"139004","DOI":"10.1016\/j.ijbiomac.2024.139004","article-title":"Use of Alfalfa Cellulose for Formulation of Strong, Biodegradable Film to Extend the Shelf Life of Strawberries","volume":"290","author":"Paudel","year":"2025","journal-title":"Int. J. Biol. Macromol."},{"key":"ref_32","doi-asserted-by":"crossref","unstructured":"Paudel, S., and Janaswamy, S. (2025). Green Valorization of Alfalfa into Sustainable Lignocellulosic Films for Packaging Applications. Appl. Sci., 15.","DOI":"10.3390\/app152211889"},{"key":"ref_33","doi-asserted-by":"crossref","first-page":"1218","DOI":"10.1039\/D5FB00211G","article-title":"Valorization of Grapevine Agricultural Waste into Transparent and High-Strength Biodegradable Films for Sustainable Packaging","volume":"3","author":"Paudel","year":"2025","journal-title":"Sustain. Food Technol."},{"key":"ref_34","doi-asserted-by":"crossref","first-page":"126798","DOI":"10.1016\/j.ijbiomac.2023.126798","article-title":"Biodegradable, UV-Blocking, and Antioxidant Films from Lignocellulosic Fibers of Spent Coffee Grounds","volume":"253","author":"Bhattarai","year":"2023","journal-title":"Int. J. Biol. Macromol."},{"key":"ref_35","doi-asserted-by":"crossref","first-page":"108443","DOI":"10.1016\/j.biombioe.2025.108443","article-title":"Valorization of Biowaste to Biopackaging: Development of Biodegradable Films from Cow Dung-Derived Cellulose","volume":"204","author":"Paudel","year":"2026","journal-title":"Biomass Bioenergy"},{"key":"ref_36","doi-asserted-by":"crossref","first-page":"20","DOI":"10.1007\/s10965-022-03397-5","article-title":"The Role of Calcium Crosslinking and Glycerol Plasticizing on the Physical and Mechanical Properties of Superabsorbent","volume":"30","author":"Abedini","year":"2023","journal-title":"J. Polym. Res."},{"key":"ref_37","doi-asserted-by":"crossref","first-page":"130601","DOI":"10.1016\/j.ijbiomac.2024.130601","article-title":"Biodegradable Films from the Lignocellulosic Fibers of Wheat Straw Biomass and the Effect of Calcium Ions","volume":"264","author":"Ahmed","year":"2024","journal-title":"Int. J. Biol. Macromol."},{"key":"ref_38","first-page":"5","article-title":"Response Surface Methodology in Experimental Design: A Comprehensive Review of Its Development, Applications, and Analytical Techniques","volume":"6","author":"Zhang","year":"2024","journal-title":"Sci. J. Technol."},{"key":"ref_39","doi-asserted-by":"crossref","unstructured":"Ohana-Levi, N., and Netzer, Y. (2025). Long-Term Global Trends in Vineyard Coverage and Fresh Grape Production. Agriculture, 15.","DOI":"10.3390\/agriculture15181976"},{"key":"ref_40","doi-asserted-by":"crossref","unstructured":"de Aguiar, A.C., Higuchi, M.T., Yamashita, F., and Roberto, S.R. (2023). SO2-Generating Pads and Packaging Materials for Postharvest Conservation of Table Grapes: A Review. Horticulturae, 9.","DOI":"10.3390\/horticulturae9060724"},{"key":"ref_41","doi-asserted-by":"crossref","first-page":"74","DOI":"10.1016\/j.postharvbio.2018.01.002","article-title":"Comparison of Postharvest UV-B and UV-C Treatments on Table Grape: Changes in Phenolic Compounds and Their Transcription of Biosynthetic Genes during Storage","volume":"138","author":"Sheng","year":"2018","journal-title":"Postharvest Biol. Technol."},{"key":"ref_42","doi-asserted-by":"crossref","first-page":"e19918","DOI":"10.1016\/j.heliyon.2023.e19918","article-title":"Effect of Calcium Spray at Flowering Combined with Post-Harvest 1-MCP Treatment on the Preservation of Grapes","volume":"9","author":"Shi","year":"2023","journal-title":"Heliyon"},{"key":"ref_43","doi-asserted-by":"crossref","first-page":"115","DOI":"10.1016\/j.jfoodeng.2010.08.001","article-title":"Effects of Passive and Active Modified Atmosphere Packaging Conditions on Ready-to-Eat Table Grape","volume":"102","author":"Costa","year":"2011","journal-title":"J. Food Eng."},{"key":"ref_44","doi-asserted-by":"crossref","first-page":"175","DOI":"10.1016\/j.scienta.2017.12.050","article-title":"Changes in the Quality and Antioxidant Components of Minimally Processed Table Grapes during Storage","volume":"232","author":"Nicolosi","year":"2018","journal-title":"Sci. Hortic."},{"key":"ref_45","doi-asserted-by":"crossref","unstructured":"Paudel, S., Regmi, S., Bhattarai, S., and Janaswamy, S. (2026). Banana Peel Waste: An Emerging Cellulosic Material for Packaging Applications. Fruit Seeds and Peels for Sustainable Biomaterials, Academic Press.","DOI":"10.1016\/B978-0-443-38329-8.00009-8"},{"key":"ref_46","doi-asserted-by":"crossref","unstructured":"Moramarco, A., Ricca, E., Acciardo, E., Laurenti, E., and Bracco, P. (2025). Cellulose Extraction from Soybean Hulls and Hemp Waste by Alkaline and Acidic Treatments: An In-Depth Investigation on the Effects of the Chemical Treatments on Biomass. Polymers, 17.","DOI":"10.3390\/polym17091220"},{"key":"ref_47","doi-asserted-by":"crossref","first-page":"274","DOI":"10.1016\/j.carbpol.2016.04.114","article-title":"A Facile Route to Prepare Cellulose-Based Films","volume":"149","author":"Xu","year":"2016","journal-title":"Carbohydr. Polym."},{"key":"ref_48","doi-asserted-by":"crossref","first-page":"116926","DOI":"10.1016\/j.indcrop.2023.116926","article-title":"Strong and Biodegradable Films from Avocado Peel Fiber","volume":"201","author":"Ahmed","year":"2023","journal-title":"Ind. Crops Prod."},{"key":"ref_49","doi-asserted-by":"crossref","first-page":"101400","DOI":"10.1016\/j.scp.2023.101400","article-title":"Biodegradable Packaging Films from Banana Peel Fiber","volume":"37","author":"Hoque","year":"2024","journal-title":"Sustain. Chem. Pharm."},{"key":"ref_50","doi-asserted-by":"crossref","unstructured":"\u0141yszczarz, E., Brniak, W., Szafraniec-Szcz\u0119sny, J., Majka, T.M., Majda, D., Zych, M., Pielichowski, K., and Jachowicz, R. (2021). The Impact of the Preparation Method on the Properties of Orodispersible Films with Aripiprazole: Electrospinning vs. Casting and 3D Printing Methods. Pharmaceutics, 13.","DOI":"10.3390\/pharmaceutics13081122"},{"key":"ref_51","doi-asserted-by":"crossref","unstructured":"Czoga\u0142a, J., Pankalla, E., and Turczyn, R. (2022). Assessments of Classical Dry-Blending\/Moulding and Solution Casting PVC Plasticization Effectiveness\u2014A Comparative Study. Res. Sq.","DOI":"10.21203\/rs.3.rs-2015602\/v1"},{"key":"ref_52","doi-asserted-by":"crossref","first-page":"2469","DOI":"10.1007\/s10570-020-02972-7","article-title":"Survey of Wheat Straw Stem Characteristics for Enhanced Resistance to Lodging","volume":"27","author":"Muhammad","year":"2020","journal-title":"Cellulose"},{"key":"ref_53","doi-asserted-by":"crossref","first-page":"124","DOI":"10.1016\/j.ijbiomac.2019.12.093","article-title":"Development and Characterization of Sodium Alginate Based Active Edible Films Incorporated with Essential Oils of Some Medicinal Plants","volume":"145","author":"Mahcene","year":"2020","journal-title":"Intl. J. Biol. Macromol."},{"key":"ref_54","doi-asserted-by":"crossref","unstructured":"Deepa, B., Abraham, E., Pothan, L.A., Cordeiro, N., Faria, M., and Thomas, S. (2016). Biodegradable Nanocomposite Films Based on Sodium Alginate and Cellulose Nanofibrils. Materials, 9.","DOI":"10.3390\/ma9010050"},{"key":"ref_55","doi-asserted-by":"crossref","first-page":"414","DOI":"10.1016\/j.foodhyd.2018.05.037","article-title":"Development and Evaluation of Chitosan Based Active Nanocomposite Films Containing Bacterial Cellulose Nanocrystals and Silver Nanoparticles","volume":"84","author":"Salari","year":"2018","journal-title":"Food Hydrocoll."},{"key":"ref_56","first-page":"100505","article-title":"Effects of Fatty Acid Esters on Mechanical, Thermal, Microbial, and Moisture Barrier Properties of Carboxymethyl Cellulose-Based Edible Films","volume":"7","author":"Mukherjee","year":"2024","journal-title":"Carbohydr. Polym. Technol. Appl."},{"key":"ref_57","doi-asserted-by":"crossref","first-page":"150274","DOI":"10.1016\/j.foodchem.2026.150274","article-title":"Cellulose-Protein Biocomposite Films with Enhanced Mechanical and Optical Properties Extend Raspberry Shelf Life","volume":"524","author":"Regmi","year":"2026","journal-title":"Food Chem."},{"key":"ref_58","doi-asserted-by":"crossref","first-page":"2309651","DOI":"10.1002\/smll.202309651","article-title":"Biodegradable, Strong, and Hydrophobic Regenerated Cellulose Films Enriched with Esterified Lignin Nanoparticles","volume":"20","author":"Tian","year":"2024","journal-title":"Small"},{"key":"ref_59","doi-asserted-by":"crossref","first-page":"119234","DOI":"10.1016\/j.carbpol.2022.119234","article-title":"Preparation of Chitosan-Cellulose-Benzyl Isothiocyanate Nanocomposite Film for Food Packaging Applications","volume":"285","author":"Jiang","year":"2022","journal-title":"Carbohydr. Polym."},{"key":"ref_60","doi-asserted-by":"crossref","first-page":"128185","DOI":"10.1016\/j.ijbiomac.2023.128185","article-title":"Impact of Soybean Protein Isolate Concentration on Chitosan-Cellulose Nanofiber Edible Films: Focus on Structure and Properties","volume":"255","author":"Qi","year":"2024","journal-title":"Int. J. Biol. Macromol."},{"key":"ref_61","doi-asserted-by":"crossref","first-page":"109491","DOI":"10.1016\/j.fbio.2026.109491","article-title":"Sustainable Soyhull-Derived Cellulose Films Reinforced with Chitosan for Improved Functional Properties","volume":"83","author":"Regmi","year":"2026","journal-title":"Food Biosci."},{"key":"ref_62","doi-asserted-by":"crossref","first-page":"140656","DOI":"10.1016\/j.ijbiomac.2025.140656","article-title":"Green Fabrication of Biodegradable Films: Harnessing the Cellulosic Residue of Oat Straw","volume":"303","author":"Ahmed","year":"2025","journal-title":"Int. J. Biol. Macromol."},{"key":"ref_63","doi-asserted-by":"crossref","first-page":"107322","DOI":"10.1016\/j.resconrec.2023.107322","article-title":"Biodegradable Films from the Lignocellulosic Residue of Switchgrass","volume":"201","author":"Bhattarai","year":"2024","journal-title":"Resour. Conserv. Recycl."},{"key":"ref_64","doi-asserted-by":"crossref","first-page":"342","DOI":"10.1021\/polymscitech.5c00024","article-title":"Ionic Crosslinking Improves the Stiffness and Toughness of Protein Hydrogels","volume":"1","author":"Fu","year":"2025","journal-title":"Polym. Sci. Technol."},{"key":"ref_65","doi-asserted-by":"crossref","unstructured":"Mohammed, A.A.B.A., Hasan, Z., Omran, A.A.B., Elfaghi, A.M., Khattak, M.A., Ilyas, R.A., and Sapuan, S.M. (2022). Effect of Various Plasticizers in Different Concentrations on Physical, Thermal, Mechanical, and Structural Properties of Wheat Starch-Based Films. Polymers, 15.","DOI":"10.3390\/polym15010063"},{"key":"ref_66","doi-asserted-by":"crossref","first-page":"101090","DOI":"10.1016\/j.fpsl.2023.101090","article-title":"Effect of Glycerol and Sorbitol on Cellulose-Based Biodegradable Films","volume":"37","author":"Paudel","year":"2023","journal-title":"Food Packag. Shelf Life"},{"key":"ref_67","doi-asserted-by":"crossref","first-page":"198","DOI":"10.1016\/j.carbpol.2015.05.040","article-title":"Edible Film Production from Chia Seed Mucilage: Effect of Glycerol Concentration on Its Physicochemical and Mechanical Properties","volume":"130","author":"Dick","year":"2015","journal-title":"Carbohydr. Polym."},{"key":"ref_68","doi-asserted-by":"crossref","unstructured":"Chandak, A., Dhull, S.B., Punia Bangar, S., and Rusu, A.V. (2022). Effects of Cross-Linking on Physicochemical and Film Properties of Lotus (Nelumbo nucifera G.) Seed Starch. Foods, 11.","DOI":"10.3390\/foods11193069"},{"key":"ref_69","doi-asserted-by":"crossref","first-page":"117427","DOI":"10.1016\/j.lwt.2025.117427","article-title":"The Effects of Glycerol Addition on the Physicochemical, Structural and Mechanical Properties of Salt-Gelatinized Rice Starch-Based Film","volume":"218","author":"Wang","year":"2025","journal-title":"LWT"},{"key":"ref_70","doi-asserted-by":"crossref","first-page":"106065","DOI":"10.1016\/j.surfin.2025.106065","article-title":"Functional Coatings with Ethyl Cellulose-Calcium Carbonate Alkaline Nanoparticles for Deacidification and Mechanical Reinforcement of Paper Artifacts","volume":"60","author":"Matej","year":"2025","journal-title":"Surf. Interfaces"},{"key":"ref_71","doi-asserted-by":"crossref","unstructured":"Razali, N.A.M., Sohaimi, R.M., Othman, R.N.I.R., Abdullah, N., Demon, S.Z.N., Jasmani, L., Yunus, W.M.Z.W., Ya\u2019acob, W.M.H.W., Salleh, E.M., and Norizan, M.N. (2022). Comparative Study on Extraction of Cellulose Fiber from Rice Straw Waste from Chemo-Mechanical and Pulping Method. Polymers, 14.","DOI":"10.3390\/polym14030387"},{"key":"ref_72","unstructured":"Niskanen, K. (2012). Packaging Performance. Mechanics of Paper Products, De Gruyter."},{"key":"ref_73","doi-asserted-by":"crossref","unstructured":"Lacroix, M. (2009). Mechanical and Permeability Properties of Edible Films and Coatings for Food and Pharmaceutical Applications. Edible Films and Coatings for Food Applications, Springer.","DOI":"10.1007\/978-0-387-92824-1_13"},{"key":"ref_74","doi-asserted-by":"crossref","first-page":"2016","DOI":"10.1021\/acs.chemrev.2c00477","article-title":"Cellulose: A Review of Water Interactions, Applications in Composites, and Water Treatment","volume":"123","author":"Etale","year":"2023","journal-title":"Chem. Rev."},{"key":"ref_75","doi-asserted-by":"crossref","first-page":"730","DOI":"10.1016\/j.jfoodeng.2005.10.007","article-title":"Equivalence of the Peleg, Pilosof and Singh\u2013Kulshrestha Models for Water Absorption in Food","volume":"78","author":"Sopade","year":"2007","journal-title":"J. Food Eng."},{"key":"ref_76","doi-asserted-by":"crossref","first-page":"114692","DOI":"10.1016\/j.indcrop.2022.114692","article-title":"Cellulosic Fraction from Agricultural Biomass as a Viable Alternative for Plastics and Plastic Products","volume":"179","author":"Janaswamy","year":"2022","journal-title":"Ind. Crops Prod."},{"key":"ref_77","doi-asserted-by":"crossref","first-page":"489","DOI":"10.1002\/col.22579","article-title":"Surface Analysis of Polymer Films for Wettability and Ink Adhesion","volume":"46","author":"Aydemir","year":"2021","journal-title":"Color Res. Appl."},{"key":"ref_78","doi-asserted-by":"crossref","first-page":"7563","DOI":"10.1021\/la2017006","article-title":"Wetting of Biopolymer Coatings: Contact Angle Kinetics and Image Analysis Investigation","volume":"27","author":"Farris","year":"2011","journal-title":"Langmuir"},{"key":"ref_79","doi-asserted-by":"crossref","first-page":"1510","DOI":"10.1007\/s13197-019-03642-8","article-title":"Evaluation of Antimicrobial and Antioxidant Activities for Cellulose Acetate Films Incorporated with Rosemary and Aloe Vera Essential Oils","volume":"56","author":"Omer","year":"2019","journal-title":"J. Food Sci. Technol."},{"key":"ref_80","doi-asserted-by":"crossref","first-page":"207","DOI":"10.1016\/j.jcs.2007.06.010","article-title":"Whole Grain Phytochemicals and Health","volume":"46","author":"Liu","year":"2007","journal-title":"J. Cereal Sci."},{"key":"ref_81","doi-asserted-by":"crossref","first-page":"910","DOI":"10.1016\/j.jff.2015.01.001","article-title":"Bioactive Phytochemicals in Wheat: Extraction, Analysis, Processing, and Functional Properties","volume":"18","author":"Luthria","year":"2015","journal-title":"J. Funct. Foods"},{"key":"ref_82","doi-asserted-by":"crossref","first-page":"860","DOI":"10.1021\/jf040456q","article-title":"Extraction and Characterization of Original Lignin and Hemicelluloses from Wheat Straw","volume":"53","author":"Sun","year":"2005","journal-title":"J. Agric. Food Chem."},{"key":"ref_83","doi-asserted-by":"crossref","first-page":"2840","DOI":"10.1007\/s12161-022-02343-x","article-title":"Film Transparency and Opacity Measurements","volume":"15","author":"Zhao","year":"2022","journal-title":"Food Anal. Methods"},{"key":"ref_84","doi-asserted-by":"crossref","first-page":"101282","DOI":"10.1016\/j.afres.2025.101282","article-title":"Study on the Selected Engineering Properties of Anchote (Coccinia abyssinia) Starch Based Biodegradable Film for Food Packaging","volume":"5","author":"Teseme","year":"2025","journal-title":"Appl. Food Res."},{"key":"ref_85","doi-asserted-by":"crossref","first-page":"105884","DOI":"10.1016\/j.foodhyd.2020.105884","article-title":"Effects of Glycerol and Thymol on Physical, Mechanical, and Thermal Properties of Corn Starch Films","volume":"106","author":"Nordin","year":"2020","journal-title":"Food Hydrocoll."},{"key":"ref_86","doi-asserted-by":"crossref","first-page":"155","DOI":"10.1016\/j.carbpol.2014.03.059","article-title":"Properties of Starch\u2013Hydroxypropyl Methylcellulose Based Films Obtained by Compression Molding","volume":"109","author":"Talens","year":"2014","journal-title":"Carbohydr. Polym."},{"key":"ref_87","doi-asserted-by":"crossref","first-page":"319","DOI":"10.1111\/j.1365-2621.2001.tb11339.x","article-title":"Physical and Mechanical Properties of Pea-Protein-Based Edible Films","volume":"66","author":"Choi","year":"2001","journal-title":"J. Food Sc."},{"key":"ref_88","doi-asserted-by":"crossref","first-page":"77","DOI":"10.1016\/j.carbpol.2015.02.004","article-title":"Mechanical and Barrier Properties of Guar Gum Based Nano-Composite Films","volume":"124","author":"Saurabh","year":"2015","journal-title":"Carbohydr. Polym."},{"key":"ref_89","doi-asserted-by":"crossref","unstructured":"Zheng, D., Zhang, Y., Guo, Y., and Yue, J. (2019). Isolation and Characterization of Nanocellulose with a Novel Shape from Walnut (Juglans regia L.) Shell Agricultural Waste. Polymers, 11.","DOI":"10.3390\/polym11071130"},{"key":"ref_90","doi-asserted-by":"crossref","first-page":"45","DOI":"10.1186\/s40643-019-0279-z","article-title":"Preparation and Characterization of Cellulose Nanocrystal Extracted from Calotropis procera Biomass","volume":"6","author":"Song","year":"2019","journal-title":"Bioresour. Bioprocess."},{"key":"ref_91","doi-asserted-by":"crossref","unstructured":"Cichosz, S., and Masek, A. (2020). IR Study on Cellulose with the Varied Moisture Contents: Insight into the Supramolecular Structure. Materials, 13.","DOI":"10.3390\/ma13204573"},{"key":"ref_92","doi-asserted-by":"crossref","unstructured":"Chieng, B.W., Lee, S.H., Ibrahim, N.A., Then, Y.Y., and Loo, Y.Y. (2017). Isolation and Characterization of Cellulose Nanocrystals from Oil Palm Mesocarp Fiber. Polymers, 9.","DOI":"10.3390\/polym9080355"},{"key":"ref_93","doi-asserted-by":"crossref","first-page":"271","DOI":"10.7569\/JRM.2017.634117","article-title":"Synthesis and Characterization of Nanocrystalline Cellulose Derived from Pineapple Peel Residues","volume":"5","author":"Camacho","year":"2017","journal-title":"J. Renew. Mater."},{"key":"ref_94","doi-asserted-by":"crossref","first-page":"106139","DOI":"10.1016\/j.foodhyd.2020.106139","article-title":"Biodegradable and Active-Intelligent Films Based on Methylcellulose and Jambol\u00e3o (Syzygium cumini) Skins Extract for Food Packaging","volume":"109","author":"Romani","year":"2020","journal-title":"Food Hydrocoll."},{"key":"ref_95","doi-asserted-by":"crossref","first-page":"108218","DOI":"10.1016\/j.fbio.2025.108218","article-title":"Alfalfa Cellulose\u2013Starch Binary Complex Films for Sustainable Biodegradable Packaging Applications","volume":"75","author":"Paudel","year":"2026","journal-title":"Food Biosci."},{"key":"ref_96","doi-asserted-by":"crossref","first-page":"473","DOI":"10.1590\/1678-457x.08817","article-title":"Water Loss in Table Grapes: Model Development and Validation under Dynamic Storage Conditions","volume":"38","author":"Pereira","year":"2018","journal-title":"Food Sci. Technol."},{"key":"ref_97","doi-asserted-by":"crossref","first-page":"112778","DOI":"10.1016\/j.postharvbio.2024.112778","article-title":"Process Parameters Optimization for Red Globe Grapes to Enhance Shelf-Life Using Non-Equilibrium Cold Plasma Jet","volume":"210","author":"Mishra","year":"2024","journal-title":"Postharvest Biol. Technol."},{"key":"ref_98","doi-asserted-by":"crossref","unstructured":"Regmi, S., Rosenau, K., Paudel, S., and Janaswamy, S. (2026). Antioxidant Active Packaging Films Based on Oat Straw Cellulose and Resveratrol for Sustainable Food Packaging. Appl. Sci., 16.","DOI":"10.3390\/app16157409"},{"key":"ref_99","doi-asserted-by":"crossref","unstructured":"Romero, I., Vazquez-Hernandez, M., Maestro-Gaitan, I., Escribano, M.I., Merodio, C., and Sanchez-Ballesta, M.T. (2020). Table Grapes during Postharvest Storage: A Review of the Mechanisms Implicated in the Beneficial Effects of Treatments Applied for Quality Retention. Int. J. Mol. Sci., 21.","DOI":"10.3390\/ijms21239320"},{"key":"ref_100","doi-asserted-by":"crossref","first-page":"15","DOI":"10.1016\/j.scienta.2011.09.021","article-title":"Postharvest Stability of Antioxidant Compounds in Hawthorn and Cornelian Cherries at Room and Refrigerator Temperatures\u2014Comparison with Blackberries, White and Red Grapes","volume":"131","year":"2011","journal-title":"Sci. Hortic."},{"key":"ref_101","doi-asserted-by":"crossref","first-page":"447","DOI":"10.17660\/ActaHortic.2008.785.59","article-title":"Effect of Storage on Physicochemical Parameters, Phenolic Compounds and Antioxidant Activity in Grapes","volume":"785","author":"Doshi","year":"2008","journal-title":"Acta Hortic."},{"key":"ref_102","doi-asserted-by":"crossref","unstructured":"Giannakourou, M.C., and Taoukis, P.S. (2021). Effect of Alternative Preservation Steps and Storage on Vitamin C Stability in Fruit and Vegetable Products: Critical Review and Kinetic Modelling Approaches. 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