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I1"],"award-info":[{"award-number":["C17. I1"]}]},{"name":"European Commission","award":["JDC2023-051979-I"],"award-info":[{"award-number":["JDC2023-051979-I"]}]},{"name":"European Commission","award":["SFRH\/BD\/150790\/2020"],"award-info":[{"award-number":["SFRH\/BD\/150790\/2020"]}]},{"name":"European Commission","award":["2024.03908.BDANA"],"award-info":[{"award-number":["2024.03908.BDANA"]}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Gels"],"abstract":"<jats:p>In the synthesis of aerogels, the influence of the drying process on the nanostructure is an issue of utmost relevance for tailoring the final properties of these materials. Among the complex parameters affecting this process, the hydrophobicity of the aerogel structure plays a key role. Thus, herein, four different silica aerogel formulations based on tetraethyl orthosilicate and trimethoxymethylsilane were employed to produce aerogels with different wettability properties (from hydrophilic samples to highly hydrophobic). The synthesized gels were dried by three methods, namely freeze-drying, high-temperature supercritical drying with ethanol, and low-temperature supercritical drying with carbon dioxide, and the influence of each procedure on bulk density, porosity, pore size, and specific surface area of the resulting aerogels was analyzed in detail. The direct correlation between the surface hydrophobicity\/hydrophilicity of the silica gels and the effects of each drying technique was analyzed, providing insights into a proper selection of the drying method depending on both the water affinity of the gel and the desired textural properties and structures.<\/jats:p>","DOI":"10.3390\/gels11070511","type":"journal-article","created":{"date-parts":[[2025,7,1]],"date-time":"2025-07-01T06:56:54Z","timestamp":1751353014000},"page":"511","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Insights on the Influence of the Drying Method and Surface Wettability on the Final Properties of Silica Aerogels"],"prefix":"10.3390","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0003-2995-6412","authenticated-orcid":false,"given":"Beatriz","family":"Merillas","sequence":"first","affiliation":[{"name":"Cellular Materials Laboratory (CellMat), Condensed Matter Physics Department, Faculty of Science, University of Valladolid, Campus Miguel Delibes, Paseo de Bel\u00e9n 7, 47011 Valladolid, Spain"},{"name":"University of Coimbra, CERES, Department of Chemical Engineering, Rua S\u00edlvio Lima, 3030-790 Coimbra, Portugal"},{"name":"BioEcoUVA Research Institute on Bioeconomy, University of Valladolid, 47011 Valladolid, Spain"},{"name":"Department of Chemistry, Faculty of Sciences, University of Burgos, 09001 Burgos, Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0014-654X","authenticated-orcid":false,"given":"Maria In\u00eas","family":"Roque","sequence":"additional","affiliation":[{"name":"University of Coimbra, CERES, Department of Chemical Engineering, Rua S\u00edlvio Lima, 3030-790 Coimbra, Portugal"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4512-7980","authenticated-orcid":false,"given":"Cl\u00e1udio M. R.","family":"Almeida","sequence":"additional","affiliation":[{"name":"University of Coimbra, CERES, Department of Chemical Engineering, Rua S\u00edlvio Lima, 3030-790 Coimbra, Portugal"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3607-690X","authenticated-orcid":false,"given":"Miguel \u00c1ngel","family":"Rodr\u00edguez-P\u00e9rez","sequence":"additional","affiliation":[{"name":"Cellular Materials Laboratory (CellMat), Condensed Matter Physics Department, Faculty of Science, University of Valladolid, Campus Miguel Delibes, Paseo de Bel\u00e9n 7, 47011 Valladolid, Spain"},{"name":"BioEcoUVA Research Institute on Bioeconomy, University of Valladolid, 47011 Valladolid, Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3336-2449","authenticated-orcid":false,"given":"Luisa","family":"Dur\u00e3es","sequence":"additional","affiliation":[{"name":"University of Coimbra, CERES, Department of Chemical Engineering, Rua S\u00edlvio Lima, 3030-790 Coimbra, Portugal"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1968","published-online":{"date-parts":[[2025,7,1]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"741","DOI":"10.1038\/127741a0","article-title":"Coherent Expanded Aerogels and Jellies","volume":"127","author":"Kistler","year":"1931","journal-title":"Nature"},{"key":"ref_2","doi-asserted-by":"crossref","first-page":"52","DOI":"10.1021\/j150331a003","article-title":"Coherent expanded aerogels","volume":"36","author":"Kistler","year":"1932","journal-title":"J. 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