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In this study, an efficient mussel shell-based adsorbent was prepared, the effects of factors (calcination temperature, calcination time, and sieved particle size) on the pyrethroid adsorption capacity from calcined shell powder were investigated via Box\u2013Behnken design, and the prediction results of the model were verified. By characterizing (scanning electron microscopy, X-ray diffraction, Fourier infrared spectroscopy, and Brunauer\u2013Emmett\u2013Teller measurements) the adsorbent before and after the optimized preparation process, the results showed that calcined shell powder had a loose and porous structure, and the main component of the shell powder under optimized condition was calcium oxide. The adsorption mechanism was also investigated, and the analysis of adsorption data showed that the Langmuir, pseudo second-order, and intra-particle diffusion models were more suitable for describing the adsorption process. The adsorbent had good adsorption potential for pyrethroids, the adsorption capacity of the two pesticides was 1.05 and 1.79 mg\/g, and the removal efficiency was over 40 and 70% at the maximum initial concentration, respectively.<\/jats:p>","DOI":"10.3390\/ma16072802","type":"journal-article","created":{"date-parts":[[2023,3,31]],"date-time":"2023-03-31T08:27:27Z","timestamp":1680251247000},"page":"2802","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":7,"title":["Adsorption of Pyrethroids in Water by Calcined Shell Powder: Preparation, Characterization, and Mechanistic Analysis"],"prefix":"10.3390","volume":"16","author":[{"given":"Xiaohan","family":"Ma","sequence":"first","affiliation":[{"name":"Key Laboratory of Food Deep Processing Technology of Animal Protein of Zhejiang Province, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"},{"name":"Zhejiang-Malaysia Joint Research Laboratory for Agricultural Product Processing and Nutrition, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Siyuan","family":"Tao","sequence":"additional","affiliation":[{"name":"Hangzhou Yuhang Food and Drug Monitoring & Testing Center, Hangzhou 311112, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shiqian","family":"Fu","sequence":"additional","affiliation":[{"name":"Key Laboratory of Food Deep Processing Technology of Animal Protein of Zhejiang Province, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"},{"name":"Zhejiang-Malaysia Joint Research Laboratory for Agricultural Product Processing and Nutrition, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Huicheng","family":"Yang","sequence":"additional","affiliation":[{"name":"Zhejiang Marine Development Research Institute, Zhoushan 316021, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bangchu","family":"Lin","sequence":"additional","affiliation":[{"name":"Zhejiang Yulin Technology Co., Ltd., Ningbo 315021, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yongjiang","family":"Lou","sequence":"additional","affiliation":[{"name":"Key Laboratory of Food Deep Processing Technology of Animal Protein of Zhejiang Province, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"},{"name":"Zhejiang-Malaysia Joint Research Laboratory for Agricultural Product Processing and Nutrition, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yongyong","family":"Li","sequence":"additional","affiliation":[{"name":"Key Laboratory of Food Deep Processing Technology of Animal Protein of Zhejiang Province, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"},{"name":"Zhejiang-Malaysia Joint Research Laboratory for Agricultural Product Processing and Nutrition, College of Food and Pharmaceutical Sciences, Ningbo University, Ningbo 315800, China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1968","published-online":{"date-parts":[[2023,3,31]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"258","DOI":"10.1016\/j.jhazmat.2016.10.056","article-title":"Global occurrence of pyrethroid insecticides in sediment and the associated toxicological effects on benthic invertebrates: An overview","volume":"324","author":"Li","year":"2017","journal-title":"J. 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