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The structure of the coatings was characterized by SEM, XRD, XPS, and AFM, as well as the corrosion resistance of the coatings by polarization curves, EIS tests, immersion tests, and salt spray tests. The conductive resistance and adhesion of different composite coatings were compared. The results demonstrate that the properties of the composite coating are significantly affected by different activation methods, and the Ni-P coating prepared with more active particles offers superior corrosion protection to the inner layer. The quantity and distribution of active particles affect the compactness of the coating by influencing the initial deposition process. The size of nickel particles is larger and the inter-grain porosity increases in the case of fewer active sites, and as the number of active sites increases, the size of nickel particles decreases, and the coating compactness increases. The mechanism of the effect of the number of active particles on the deposition process of electroless Ni-P coating was proposed.<\/jats:p>","DOI":"10.3390\/ma16186185","type":"journal-article","created":{"date-parts":[[2023,9,13]],"date-time":"2023-09-13T05:31:28Z","timestamp":1694583088000},"page":"6185","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Effect of Surface Activation on the Microstructure and Corrosion Resistance of MAO\/Ni-P Composite Coating on AZ91D Magnesium Alloy"],"prefix":"10.3390","volume":"16","author":[{"given":"Qi","family":"Xu","sequence":"first","affiliation":[{"name":"Shenyang National Laboratory for Materials Science, Northeastern University, 3-11 Wenhua Road, Shenyang 110819, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Peng","family":"Zhou","sequence":"additional","affiliation":[{"name":"Shenyang National Laboratory for Materials Science, Northeastern University, 3-11 Wenhua Road, Shenyang 110819, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tao","family":"Zhang","sequence":"additional","affiliation":[{"name":"Shenyang National Laboratory for Materials Science, Northeastern University, 3-11 Wenhua Road, Shenyang 110819, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fuhui","family":"Wang","sequence":"additional","affiliation":[{"name":"Shenyang National Laboratory for Materials Science, Northeastern University, 3-11 Wenhua Road, Shenyang 110819, China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1968","published-online":{"date-parts":[[2023,9,13]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"2898","DOI":"10.1016\/j.electacta.2005.08.026","article-title":"Electrochemical corrosion behavior of composite coatings of sealed MAO film on magnesium alloy AZ91D","volume":"51","author":"Duan","year":"2006","journal-title":"Electrochim. 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