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As part of this effort, heat treatment was explored. This study compares the microstructure and mechanical properties of the as-printed sample with those cooled in water after undergoing heat treatment at temperatures ranging from 1000 to 1200 \u00b0C for 1 h. Both pre- and post-treatment samples reveal a dual-phase microstructure comprising FCC and BCC phases. Although heat treatment led to a reduction in tensile and yield strength, it significantly increased ductility compared to the as-printed sample. This strength-ductility trade-off is related to changes in grain sizes with ultrafine grains enhancing strength and micron grains optimizing ductility, also influencing the content of FCC\/BCC phases and dislocation density. In particular, the sample heat-treated at 1000 \u00b0C for 1 h and then water-cooled exhibited a better combination of strength and ductility, a yield strength of 790 MPa, and an elongation of 13%. This research offers innovative perspectives on crafting dual-phase HEA of Fe32Cr33Ni29Al3Ti3, allowing for tailorable microstructure and mechanical properties through a synergistic approach involving LB-PBF and heat treatment.<\/jats:p>","DOI":"10.3390\/mi15040471","type":"journal-article","created":{"date-parts":[[2024,3,31]],"date-time":"2024-03-31T13:42:30Z","timestamp":1711892550000},"page":"471","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["Effects of Heat Treatment on the Microstructure and Mechanical Properties of a Dual-Phase High-Entropy Alloy Fabricated via Laser Beam Power Bed Fusion"],"prefix":"10.3390","volume":"15","author":[{"ORCID":"https:\/\/orcid.org\/0009-0009-3697-162X","authenticated-orcid":false,"given":"Xiaojun","family":"Tan","sequence":"first","affiliation":[{"name":"Guangdong Provincial Key Laboratory of Nanophotonic Functional Materials and Devices, School of Information and Optoelectronic Science and Engineering, South China Normal University, Guangzhou 510006, China"},{"name":"Sino-German Intelligent Manufacturing School, Shenzhen Institute of Technology, Shenzhen 518116, China"},{"name":"Intelligent Manufacturing and Equipment School, Shenzhen Institute of Information Technology, Shenzhen 518172, China"},{"name":"Guangdong Provincial Key Laboratory of Industrial Ultrashort Pulse Laser Technology, Shenzhen 518055, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zihong","family":"Wang","sequence":"additional","affiliation":[{"name":"College of Materials Science and Engineering, Chongqing University, Chongqing 400045, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Haitao","family":"Chen","sequence":"additional","affiliation":[{"name":"Sino-German Intelligent Manufacturing School, Shenzhen Institute of Technology, Shenzhen 518116, 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