{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,4,8]],"date-time":"2026-04-08T17:19:11Z","timestamp":1775668751170,"version":"3.50.1"},"reference-count":79,"publisher":"MDPI AG","issue":"11","license":[{"start":{"date-parts":[[2012,11,8]],"date-time":"2012-11-08T00:00:00Z","timestamp":1352332800000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/3.0\/"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Molecules"],"abstract":"<jats:p>Six silver(I) coordination complexes have been prepared and structurally characterised. Mixed chalcogen-donor acenaphthene ligands L1\u2013L3 [Acenap(EPh)(E'Ph)] (Acenap = acenaphthene-5,6-diyl; E\/E' = S, Se, Te) were independently treated with silver(I) salts (AgBF4\/AgOTf). In order to keep the number of variables to a minimum, all reactions were carried out using a 1:1 ratio of Ag\/L and run in dichloromethane. The nature of the donor atoms, the coordinating ability of the respective counter-anion and the type of solvent used in recrystallisation, all affect the structural architecture of the final silver(I) complex, generating monomeric, silver(I) complexes {[AgBF4(L)2] (1 L = L1; 2 L = L2; 3 L = L3), [AgOTf(L)3] (4 L = L1; 5 L = L3), [AgBF4(L)3] (2a L = L1; 3a L = L3)} and a 1D polymeric chain {[AgOTf(L3)]n 6}. The organic acenaphthene ligands L1-L3 adopt a number of ligation modes (bis-monodentate \u03bc2-\u03b72-bridging, quasi-chelating combining monodentate and \u03b76-E(phenyl)-Ag(I) and classical monodentate coordination) with the central silver atom at the centre of a tetrahedral or trigonal planar coordination geometry in each case. The importance of weak interactions in the formation of metal-organic structures is also highlighted by the number of short non-covalent contacts present within each complex.<\/jats:p>","DOI":"10.3390\/molecules171113307","type":"journal-article","created":{"date-parts":[[2012,11,8]],"date-time":"2012-11-08T11:04:29Z","timestamp":1352372669000},"page":"13307-13329","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":9,"title":["Investigating Silver Coordination to Mixed Chalcogen Ligands"],"prefix":"10.3390","volume":"17","author":[{"given":"Fergus R.","family":"Knight","sequence":"first","affiliation":[{"name":"EaStCHEM School of Chemistry, University of St. Andrews, St Andrews, Fife KY16 9ST, UK"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Rebecca A. M.","family":"Randall","sequence":"additional","affiliation":[{"name":"EaStCHEM School of Chemistry, University of St. Andrews, St Andrews, Fife KY16 9ST, UK"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Lucy","family":"Wakefield","sequence":"additional","affiliation":[{"name":"EaStCHEM School of Chemistry, University of St. Andrews, St Andrews, Fife KY16 9ST, UK"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Alexandra M. Z.","family":"Slawin","sequence":"additional","affiliation":[{"name":"EaStCHEM School of Chemistry, University of St. Andrews, St Andrews, Fife KY16 9ST, UK"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"J. Derek","family":"Woollins","sequence":"additional","affiliation":[{"name":"EaStCHEM School of Chemistry, University of St. Andrews, St Andrews, Fife KY16 9ST, UK"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"1968","published-online":{"date-parts":[[2012,11,8]]},"reference":[{"key":"ref_1","unstructured":"Cotton, F.A., and Wilkinson, G. (1988). Advanced Inorganic Chemistry, Wiley. [5th]."},{"key":"ref_2","unstructured":"Greenwood, N.N., and Earnshaw, A. (1984). Chemistry of the Elements, Pergamon. [2nd]."},{"key":"ref_3","unstructured":"Shriver, D.F., and Atkins, P.W. (1990). Inorganic Chemistry, Oxford University Press. [3rd]."},{"key":"ref_4","doi-asserted-by":"crossref","first-page":"915","DOI":"10.1021\/ed074p915","article-title":"A Coordination Geometry Table of the d-Block Elements and Their Ions","volume":"74","author":"Venkataraman","year":"1997","journal-title":"J. Chem. Educ."},{"key":"ref_5","doi-asserted-by":"crossref","first-page":"293","DOI":"10.1016\/0010-8545(93)80036-5","article-title":"One-dimensional coordination polymers: Applications to material science","volume":"128","author":"Chen","year":"1993","journal-title":"Coord. Chem. Rev."},{"key":"ref_6","doi-asserted-by":"crossref","first-page":"1151","DOI":"10.1021\/ja00082a055","article-title":"Preparation, Clathration Ability, and Catalysis of a Two-Dimensional Square Network Material Composed of Cadmium(II) and 4,4'-Bipyridine","volume":"116","author":"Fujita","year":"1994","journal-title":"J. Am. Chem. Soc."},{"key":"ref_7","doi-asserted-by":"crossref","first-page":"1546","DOI":"10.1021\/ja00160a038","article-title":"Design and construction of a new class of scaffolding-like materials comprising infinite polymeric frameworks of 3D-linked molecular rods. A reappraisal of the zinc cyanide and cadmium cyanide structures and the synthesis and structure of the diamond-related frameworks [N(CH3)4][CuIZnII(CN)4] and CuI[4,4',4'',4'''-tetracyanotetraphenylmethane]BF4.xC6H5NO2","volume":"112","author":"Hoskins","year":"1990","journal-title":"J. Am. Chem. Soc."},{"key":"ref_8","doi-asserted-by":"crossref","first-page":"4562","DOI":"10.1021\/ja00121a014","article-title":"1-, 2-, and 3-Dimensional polymeric frames in the coordination chemistry of AgBF4 with pyrazine. The first example of three interpenetrating 3-dimensional triconnected nets","volume":"117","author":"Carlucci","year":"1995","journal-title":"J. Am. Chem. Soc."},{"key":"ref_9","doi-asserted-by":"crossref","first-page":"792","DOI":"10.1038\/374792a0","article-title":"Spontaneous assembly of a hinged coordination network","volume":"374","author":"Gardner","year":"1995","journal-title":"Nature"},{"key":"ref_10","doi-asserted-by":"crossref","first-page":"1710","DOI":"10.1021\/om2000162","article-title":"Silver(I)-Organic Networks Assembled with Propargyl-Functionalized Di- and Trihydroxybenzenes","volume":"30","author":"Li","year":"2011","journal-title":"Organometallics"},{"key":"ref_11","doi-asserted-by":"crossref","first-page":"464","DOI":"10.1039\/B416576B","article-title":"Novel dithioether-silver(I) coordination architectures: Structural diversities by varying the spacers and terminal groups of ligands","volume":"2005","author":"Li","year":"2005","journal-title":"Dalton Trans."},{"key":"ref_12","doi-asserted-by":"crossref","first-page":"5483","DOI":"10.1039\/c1dt10029g","article-title":"Silvercoordination networks and cages based on a semi-rigid bis(isoxazoylyl)ligand","volume":"40","author":"Burrows","year":"2011","journal-title":"Dalton Trans."},{"key":"ref_13","doi-asserted-by":"crossref","first-page":"3477","DOI":"10.1021\/ic0113045","article-title":"Controlling the Framework Formation of Silver(I) Coordination Polymers with 1,4-Bis(phenylthio)butane by Varying the Solvents, Metal-to-Ligand Ratio, and Counteranions","volume":"41","author":"Bu","year":"2002","journal-title":"Inorg. Chem."},{"key":"ref_14","doi-asserted-by":"crossref","first-page":"501","DOI":"10.1023\/B:JOCC.0000042017.66254.05","article-title":"Synthesis and crystal structure of a 2D (6,3) coordination network, {[Ag(L)1.5]NO3}n [L = 1,3-bis(benzylthio)propane]","volume":"34","author":"Li","year":"2004","journal-title":"J. Chem. Crystallogr."},{"key":"ref_15","doi-asserted-by":"crossref","first-page":"3493","DOI":"10.1039\/a703636a","article-title":"Synthesis and characterisation of transition-metal complexes involving cyclic diselenoether ligands","volume":"1997","author":"Booth","year":"1997","journal-title":"Dalton Trans."},{"key":"ref_16","doi-asserted-by":"crossref","first-page":"1346","DOI":"10.1016\/j.ccr.2007.07.017","article-title":"Square planar silver(I) complexes: A rare but increasingly observed stereochemistry for silver(I)","volume":"252","author":"Young","year":"2008","journal-title":"Coord. Chem. Rev."},{"key":"ref_17","doi-asserted-by":"crossref","first-page":"771","DOI":"10.1002\/ejic.200700930","article-title":"The Use of 2,1,3-Benzoselenadiazole as an Auxiliary Ligand for the Construction of New 2D Silver(I)\/Benzene- or Cyclohexane-1,3,5-tricarboxylate Honeycomb Networks","volume":"2008","author":"Tan","year":"2008","journal-title":"Eur. J. Inorg. Chem."},{"key":"ref_18","doi-asserted-by":"crossref","first-page":"306","DOI":"10.1098\/rspa.1951.0119","article-title":"Bond Lengths in Naphthalene and Anthracene","volume":"207","author":"Coulson","year":"1951","journal-title":"Proc. R. Soc. London Ser. A"},{"key":"ref_19","doi-asserted-by":"crossref","first-page":"504","DOI":"10.1107\/S0365110X57001826","article-title":"A Detailed Refinement of the Crystal and Molecular Structure of Naphthalene","volume":"10","author":"Cruickshank","year":"1957","journal-title":"Acta Crystallogr."},{"key":"ref_20","doi-asserted-by":"crossref","first-page":"2218","DOI":"10.1107\/S0567740882008358","article-title":"Temperature Dependence of Thermal Motion in Crystalline Naphthalene","volume":"38","author":"Brock","year":"1982","journal-title":"Acta Crystallogr. B"},{"key":"ref_21","doi-asserted-by":"crossref","first-page":"1057","DOI":"10.1021\/jp036186g","article-title":"Charge Density Study of Naphthalene Based on X-ray Diffraction Data at Four Different Temperatures and Theoretical Calculations","volume":"108","author":"Oddershede","year":"2004","journal-title":"J. Phys. Chem. A"},{"key":"ref_22","doi-asserted-by":"crossref","first-page":"690","DOI":"10.1107\/S0108270186094908","article-title":"A neutron diffraction study of the crystal and molecular structure of acenaphthene","volume":"42","author":"Hazell","year":"1986","journal-title":"Acta Crystallogr. C"},{"key":"ref_23","doi-asserted-by":"crossref","first-page":"2302","DOI":"10.1002\/chem.201001750","article-title":"Naphthalene and Related Systems peri-Substituted by Group 15 and 16 Elements","volume":"17","author":"Kilian","year":"2011","journal-title":"Chem. Eur. J."},{"key":"ref_24","doi-asserted-by":"crossref","first-page":"1387","DOI":"10.1016\/j.ccr.2011.01.015","article-title":"Synthesis of ligands based on naphthalene peri-substituted by Group 15 and 16 elements and their coordination chemistry","volume":"255","author":"Kilian","year":"2011","journal-title":"Coord. Chem. Rev."},{"key":"ref_25","doi-asserted-by":"crossref","first-page":"1666","DOI":"10.1002\/chem.200305352","article-title":"Platinum Complexes of Naphthalene-1,8-dichalcogen and Related Polyaromatic Hydrocarbon Ligands","volume":"10","author":"Aucott","year":"2004","journal-title":"Chem. Eur. J."},{"key":"ref_26","doi-asserted-by":"crossref","first-page":"531","DOI":"10.1002\/hc.20055","article-title":"Crystal Structures and Molecular Modelling Of 1,8 Chalcogenide Substituted Naphthalenes","volume":"15","author":"Aucott","year":"2004","journal-title":"Heteroat. Chem."},{"key":"ref_27","doi-asserted-by":"crossref","first-page":"3347","DOI":"10.1039\/b409700a","article-title":"The preparation and characterisation of bimetallic Iridium(II) complexes containing derivatised bridging naphthalene-1,8-disulfur or 4,5-dithiolato acephenanthrylene ligands","volume":"2004","author":"Aucott","year":"2004","journal-title":"Dalton Trans."},{"key":"ref_28","doi-asserted-by":"crossref","first-page":"2710","DOI":"10.1021\/ic048483l","article-title":"Bis(cyclopentadienyl)titanium complexes of naphthalene-1,8-dithiolates, biphenyl 2,2' dithiolates and related ligands","volume":"44","author":"Aucott","year":"2005","journal-title":"Inorg. Chem."},{"key":"ref_29","doi-asserted-by":"crossref","first-page":"895","DOI":"10.1002\/chem.200500446","article-title":"Platinum Complexes of Dibenzo[1,2]dithiine and Related Polyaromatic Hydrocarbon Ligands","volume":"12","author":"Aucott","year":"2006","journal-title":"Chem. Eur. J."},{"key":"ref_30","doi-asserted-by":"crossref","first-page":"5495","DOI":"10.1002\/chem.200600205","article-title":"The Preparation and Characterisation of Hetero and Homo-bimetallic Complexes Containing Bridging Naphthalene-1,8-dithiolato Ligands","volume":"12","author":"Aucott","year":"2006","journal-title":"Chem. Eur. J."},{"key":"ref_31","doi-asserted-by":"crossref","first-page":"3876","DOI":"10.1039\/b310392g","article-title":"A structural study of 1,8-Bis(dimethyl phosphonito) naphthalene and related crowded chalcogeno derivatives","volume":"2003","author":"Kilian","year":"2003","journal-title":"Dalton Trans."},{"key":"ref_32","doi-asserted-by":"crossref","first-page":"249","DOI":"10.1002\/ejic.200390033","article-title":"Use of Molecular Scaffolding for the Stabilization of an Intramolecular Dative PIII\u2013PV System","volume":"2003","author":"Kilian","year":"2003","journal-title":"Eur. J. Inorg. Chem."},{"key":"ref_33","doi-asserted-by":"crossref","first-page":"215","DOI":"10.1002\/chem.200390015","article-title":"Naphthalene-1,8-diyl Bis(Halogenophosphanes): Novel Syntheses and Structures of Useful Synthetic Building Blocks","volume":"9","author":"Kilian","year":"2003","journal-title":"Chem. Eur. J."},{"key":"ref_34","doi-asserted-by":"crossref","first-page":"1174","DOI":"10.1039\/b301601c","article-title":"New Mode of Sterically imposed Hypercoordination","volume":"2003","author":"Kilian","year":"2003","journal-title":"Chem. Commun."},{"key":"ref_35","doi-asserted-by":"crossref","first-page":"2252","DOI":"10.1021\/ic035364h","article-title":"Chlorides, oxochlorides and oxoacids of 1,8-diphospha naphthalene - A system with enforced close P\u00b7\u00b7\u00b7P interaction","volume":"43","author":"Kilian","year":"2004","journal-title":"Inorg. Chem."},{"key":"ref_36","doi-asserted-by":"crossref","first-page":"1719","DOI":"10.1016\/j.ica.2004.09.019","article-title":"Phosphonato-phosphinito peri-substituted naphthalenes","volume":"358","author":"Kilian","year":"2005","journal-title":"Inorg. Chim. Acta"},{"key":"ref_37","doi-asserted-by":"crossref","first-page":"2175","DOI":"10.1039\/b517071k","article-title":"Preparation and structures of 1,2-dihydro-1,2-diphosphaacenaphthenes and rigid backbone stabilised triphosphenium cation","volume":"2006","author":"Kilian","year":"2006","journal-title":"Dalton Trans."},{"key":"ref_38","doi-asserted-by":"crossref","first-page":"7503","DOI":"10.1002\/chem.200903523","article-title":"Synthetic and Structural Studies of 1,8-Chalcogen Naphthalene Derivatives","volume":"16","author":"Knight","year":"2010","journal-title":"Chem. Eur. J."},{"key":"ref_39","doi-asserted-by":"crossref","first-page":"7605","DOI":"10.1002\/chem.201000435","article-title":"Synthetic and Structural Studies of 1-Halo-8-(alkylchalcogeno)naphthalene Derivatives","volume":"16","author":"Knight","year":"2010","journal-title":"Chem. Eur. J."},{"key":"ref_40","doi-asserted-by":"crossref","first-page":"7577","DOI":"10.1021\/ic101086h","article-title":"Hypervalent Adducts of Chalcogen-Containing peri-Substituted Naphthalenes; Reactions of Sulfur, Selenium, and Tellurium with Dihalogens","volume":"49","author":"Knight","year":"2010","journal-title":"Inorg. Chem."},{"key":"ref_41","doi-asserted-by":"crossref","first-page":"o3855","DOI":"10.1107\/S1600536807040627","article-title":"1-Bromo-8-(phenylselenyl)naphthalene","volume":"E63","author":"Fuller","year":"2007","journal-title":"Acta Crystallogr. E"},{"key":"ref_42","doi-asserted-by":"crossref","first-page":"o3957","DOI":"10.1107\/S1600536807042432","article-title":"1-Bromo-8-(ethylsulfanyl)naphthalene","volume":"E63","author":"Fuller","year":"2007","journal-title":"Acta Crystallogr. E"},{"key":"ref_43","doi-asserted-by":"crossref","first-page":"o977","DOI":"10.1107\/S1600536808012580","article-title":"8-Bromonaphthalen-1-amine","volume":"E64","author":"Fuller","year":"2008","journal-title":"Acta Crystallogr. E"},{"key":"ref_44","doi-asserted-by":"crossref","first-page":"8476","DOI":"10.1039\/b916692k","article-title":"Controlling Cu\u00b7\u00b7\u00b7Cu distances using halides: (8-Phenylthionaphth-1-yl)diphenylphosphine copper halide dimers","volume":"2009","author":"Knight","year":"2009","journal-title":"Dalton Trans."},{"key":"ref_45","doi-asserted-by":"crossref","first-page":"1849","DOI":"10.1016\/j.poly.2010.02.033","article-title":"Preparation and compounds of (8-methoxynaphth-1-yl)diphenylphosphine","volume":"29","author":"Knight","year":"2010","journal-title":"Polyhedron"},{"key":"ref_46","doi-asserted-by":"crossref","first-page":"1956","DOI":"10.1016\/j.poly.2010.03.006","article-title":"Synthesis and structural study of (8-phenylsulfanylnaphth-1-yl)diphenylphosphine metal complexes","volume":"29","author":"Knight","year":"2010","journal-title":"Polyhedron"},{"key":"ref_47","doi-asserted-by":"crossref","first-page":"7617","DOI":"10.1002\/chem.201000454","article-title":"Sterically Crowded peri-Substituted Naphthalene Phosphines and their PV Derivatives","volume":"16","author":"Knight","year":"2010","journal-title":"Chem. Eur. J."},{"key":"ref_48","doi-asserted-by":"crossref","first-page":"4034","DOI":"10.1002\/ejic.201000357","article-title":"Platinum Complexes of Aromatic Selenolates","volume":"2010","author":"Fuller","year":"2010","journal-title":"Eur. J. Inorg. Chem."},{"key":"ref_49","doi-asserted-by":"crossref","first-page":"3141","DOI":"10.1039\/C1DT11697E","article-title":"Onset of three-centre, four-electron bonding in peri-substituted acenaphthenes: A structural and computational investigation","volume":"41","author":"Aschenbach","year":"2012","journal-title":"Dalton Trans."},{"key":"ref_50","doi-asserted-by":"crossref","first-page":"3154","DOI":"10.1039\/c2dt12031c","article-title":"Exploring hypervalency and three-centre, four-electron bonding interactions: Reactions of acenaphthene chalcogen donors and dihalogen acceptors","volume":"41","author":"Knight","year":"2012","journal-title":"Dalton Trans."},{"key":"ref_51","doi-asserted-by":"crossref","first-page":"11087","DOI":"10.1021\/ic301627y","article-title":"Noncovalent Interactions in Peri-Substituted Chalconium Acenaphthene and Naphthalene Salts: A Combined Experimental, Crystallographic, Computational, and Solid-State NMR Study","volume":"51","author":"Knight","year":"2012","journal-title":"Inorg. Chem."},{"key":"ref_52","doi-asserted-by":"crossref","first-page":"2922","DOI":"10.1021\/om201253t","article-title":"Sterically Crowded Tin Acenaphthenes","volume":"31","author":"Lechner","year":"2012","journal-title":"Organometallics"},{"key":"ref_53","doi-asserted-by":"crossref","unstructured":"Knight, F.R., Randall, R.M., Wakefield, L., Slawin, A.M.Z., and Woollins, J.D. (2013). Silver(I) coordination complexes and extended networks assembled from S, Se, Te substituted acenaphthenes. Dalton Trans.","DOI":"10.1039\/C2DT31390A"},{"key":"ref_54","unstructured":"Knight, F.R., Randall, R.M., Wakefield, L., Slawin, A.M.Z., and Woollins, J.D. (2012). University of St Andrews, St Andrews, Fife, UK. Unpublished work."},{"key":"ref_55","doi-asserted-by":"crossref","first-page":"441","DOI":"10.1021\/j100785a001","article-title":"Van der Waals Volumes and Radii","volume":"68","author":"Bondi","year":"1964","journal-title":"J. Phys. Chem."},{"key":"ref_56","doi-asserted-by":"crossref","first-page":"371","DOI":"10.1039\/cc9960000371","article-title":"Structure of bis[8-(phenylselanyl)naphthyl] diselenide: First linear alignment of four Se atoms as a four-centre six-electron bond","volume":"1996","author":"Nakanishi","year":"1996","journal-title":"Chem. Commun."},{"key":"ref_57","doi-asserted-by":"crossref","first-page":"3635","DOI":"10.1021\/ja974070q","article-title":"Attraxtive Interaction Caused by the Linear F\u00b7\u00b7\u00b7Se-C Alignment in Naphthalene Peri Positions","volume":"120","author":"Nakanishi","year":"1998","journal-title":"J. Am. Chem. Soc."},{"key":"ref_58","doi-asserted-by":"crossref","first-page":"8790","DOI":"10.1021\/jo980885l","article-title":"Four-Center Six-Electron Interaction versus Lone Pair-Lone Pair Interaction between Selenium Atoms in Naphthalene Peri Positions","volume":"63","author":"Nakanishi","year":"1998","journal-title":"J. Org. Chem."},{"key":"ref_59","doi-asserted-by":"crossref","first-page":"6688","DOI":"10.1021\/jo9903860","article-title":"Novel Substituent Effect on 77Se-NMR Chemical Shifts Caused by 4c-6e versus 2c-4e and 3c-4e in Naphthalene Peri Positions: Spectroscopic and Theoretical Study","volume":"64","author":"Hayashi","year":"1999","journal-title":"J. Org. Chem."},{"key":"ref_60","doi-asserted-by":"crossref","first-page":"9906","DOI":"10.1021\/jp991910+","article-title":"Successive Change in Conformation Caused by p-Y Groups in 1-(MeSe)-8-(p-YC6H4Se)C10H6: Role of Linear Se\u00b7\u00b7\u00b7Se-C Three-Center-Four-Electron versus n(Se)\u00b7\u00b7\u00b7n(Se) Two-Center-Four-Electron Nonbonded Interactions","volume":"103","author":"Nakanishi","year":"1999","journal-title":"J. Phys. Chem. A"},{"key":"ref_61","doi-asserted-by":"crossref","first-page":"3933","DOI":"10.1002\/1099-0690(200110)2001:20<3933::AID-EJOC3933>3.0.CO;2-L","article-title":"Structure of 1-(Arylselanyl)naphthalenes\u2014Y Dependence in 1-(p-YC6H4Se)C10H7","volume":"2001","author":"Nakanishi","year":"2001","journal-title":"Eur. J. Org. Chem."},{"key":"ref_62","doi-asserted-by":"crossref","first-page":"1833","DOI":"10.1080\/10426500212208","article-title":"Nonbonded P\u00b7\u00b7\u00b7P and P\u00b7\u00b7\u00b7Se Interactions in Naphthalene 1,8-Positions: Role of Lone-Pair Orbitals","volume":"177","author":"Nakanishi","year":"2002","journal-title":"Phosphorus Sulfur Silicon Relat. Elem."},{"key":"ref_63","doi-asserted-by":"crossref","first-page":"2416","DOI":"10.1039\/b206137f","article-title":"Linear alignment of four sulphur atoms in bis[(8-phenylthio)naphthyl] disulfude: Contribution of linear S4 hypervalent four-centre six-electron bond to the structure","volume":"2002","author":"Nakanishi","year":"2002","journal-title":"Chem. Commun."},{"key":"ref_64","doi-asserted-by":"crossref","first-page":"38","DOI":"10.1021\/jo010380m","article-title":"Structure of 1-(Arylselanyl)naphthalenes. 2. G Dependence in 8-G-1-(p-YC6H4Se)C10H6","volume":"67","author":"Hayashi","year":"2002","journal-title":"J. Org. Chem."},{"key":"ref_65","doi-asserted-by":"crossref","first-page":"124","DOI":"10.1039\/B209261A","article-title":"First linear alignment of five C-Se\u00b7\u00b7\u00b7O\u00b7\u00b7\u00b7Se-C atoms in anthraquinone and 9-(methoxy)anthracene bearing phenylselanyl groups at 1,8-positions","volume":"2003","author":"Nakanishi","year":"2003","journal-title":"Chem. Commun."},{"key":"ref_66","doi-asserted-by":"crossref","first-page":"5574","DOI":"10.1021\/jo060527f","article-title":"Structures of 1-(Arylseleninyl)naphthalenes: O, G, and Y Dependences in 8-G-1-[p-YC6H4Se(O)]C10H6","volume":"71","author":"Hayashi","year":"2006","journal-title":"J. Org. Chem."},{"key":"ref_67","doi-asserted-by":"crossref","first-page":"1605","DOI":"10.1246\/bcsj.81.1605","article-title":"Noncovalent Z\u00b7\u00b7\u00b7Z (Z = O, S, Se and Te) Interactions: How Do They Operate to Control Fine Structures of 1,8-Dichalcogene-Substituted Naphthalenes","volume":"81","author":"Hayashi","year":"2008","journal-title":"Bull. Chem. Soc. Jpn."},{"key":"ref_68","doi-asserted-by":"crossref","first-page":"61","DOI":"10.1016\/S0022-2860(01)00821-3","article-title":"Intramolecular S\u22efS and S\u22efO close contacts in 1,8-bis(phenylsulfanyl)naphthalene derivatives of different sulfur valence state: An X-ray study","volume":"606","author":"Nagy","year":"2002","journal-title":"J. Mol. Struct."},{"key":"ref_69","doi-asserted-by":"crossref","first-page":"130","DOI":"10.1039\/b313104a","article-title":"CH\/\u03c0 hydrogen bonds in crystals","volume":"6","author":"Nishio","year":"2004","journal-title":"CrystEngComm."},{"key":"ref_70","doi-asserted-by":"crossref","first-page":"o673","DOI":"10.1107\/S1600536808002304","article-title":"5,11,17,23-Tetra-tert-butyl-25,26,27,28-tetramethoxycalix[4]arene dichloromethane hemisolvate","volume":"E64","author":"Fischer","year":"2008","journal-title":"Acta Crystallogr. Sec. E"},{"key":"ref_71","doi-asserted-by":"crossref","first-page":"620","DOI":"10.1002\/1099-1395(200010)13:10<620::AID-POC262>3.0.CO;2-F","article-title":"Intramolecular CH-\u03c0 interaction. Substituent effect as a probe for hydrogen bond-like character","volume":"13","author":"Hirota","year":"2000","journal-title":"J. Phys. Org. Chem."},{"key":"ref_72","doi-asserted-by":"crossref","first-page":"385","DOI":"10.1039\/B407947G","article-title":"Effect of intramolecular \u03c0-\u03c0 and CH\u2013\u03c0 interactions between ligands on structure, electrochemical and spectroscopic properties of fac-[Re(bpy)(CO)3(PR3)]+ (bpy = 2,2'-bipyridine; PR3 = trialkyl or triarylphosphines)","volume":"2005","author":"Tsubaki","year":"2005","journal-title":"Dalton Trans."},{"key":"ref_73","doi-asserted-by":"crossref","first-page":"7","DOI":"10.1107\/S0021889802022112","article-title":"Single-crystal structure validation with the program PLATON","volume":"36","author":"Spek","year":"2003","journal-title":"J. Appl. Cryst."},{"key":"ref_74","doi-asserted-by":"crossref","first-page":"148","DOI":"10.1107\/S090744490804362X","article-title":"Structure validation in chemical crystallography","volume":"65","author":"Spek","year":"2009","journal-title":"Acta Crystallogr. D"},{"key":"ref_75","unstructured":"(Acta Crystallogr. D, 1999). Rigaku Corporation, 2010. CrystalClear Software User\u2019s Guide, Molecular Structure Corporation, \u00a9 2000. Flugrath, J.W.P. The finer things in X-ray diffraction data collection, Acta Crystallogr. D."},{"key":"ref_76","doi-asserted-by":"crossref","first-page":"115","DOI":"10.1107\/S0021889898007717","article-title":"SIR97: A new tool for crystal structure determination and refinement","volume":"32","author":"Altomare","year":"1999","journal-title":"J. Appl. Cryst."},{"key":"ref_77","unstructured":"Beurskens, P.T., Admiraal, G., Beurskens, G., Bosman, W.P., de Gelder, R., Israel, R., and Smits, J.M.M. (1999). The DIRDIF-99 Program System, Technical Report of the Crystallography Laboratory, University of Nijmegen. DIRDIF99."},{"key":"ref_78","unstructured":"CrystalStructure 4.0, Crystal Structure Analysis Package, Rigaku and Rigaku\/MSC (2009). 9009 New Trails Dr., The Woodlands, TX 77381, USA."},{"key":"ref_79","doi-asserted-by":"crossref","first-page":"112","DOI":"10.1107\/S0108767307043930","article-title":"A short history of SHELX","volume":"64","author":"Sheldrick","year":"2008","journal-title":"Acta Crystallogr. A"}],"container-title":["Molecules"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/www.mdpi.com\/1420-3049\/17\/11\/13307\/pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,10,11]],"date-time":"2025-10-11T21:53:25Z","timestamp":1760219605000},"score":1,"resource":{"primary":{"URL":"https:\/\/www.mdpi.com\/1420-3049\/17\/11\/13307"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2012,11,8]]},"references-count":79,"journal-issue":{"issue":"11","published-online":{"date-parts":[[2012,11]]}},"alternative-id":["molecules171113307"],"URL":"https:\/\/doi.org\/10.3390\/molecules171113307","relation":{},"ISSN":["1420-3049"],"issn-type":[{"value":"1420-3049","type":"electronic"}],"subject":[],"published":{"date-parts":[[2012,11,8]]}}}