{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,12,1]],"date-time":"2025-12-01T11:21:07Z","timestamp":1764588067810,"version":"build-2065373602"},"reference-count":33,"publisher":"MDPI AG","issue":"21","license":[{"start":{"date-parts":[[2019,11,4]],"date-time":"2019-11-04T00:00:00Z","timestamp":1572825600000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100010198","name":"Ministerio de Econom\u00eda, Industria y Competitividad, Gobierno de Espa\u00f1a","doi-asserted-by":"publisher","award":["CTQ2016-78289-P"],"award-info":[{"award-number":["CTQ2016-78289-P"]}],"id":[{"id":"10.13039\/501100010198","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100018647","name":"RUDN University","doi-asserted-by":"publisher","award":["Program 5-100"],"award-info":[{"award-number":["Program 5-100"]}],"id":[{"id":"10.13039\/501100018647","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Molecules"],"abstract":"<jats:p>In this study, the co-synthesis of TiO2 and Cu metallic nanoparticles obtained via one-pot cost-efficient hydrothermal process has been addressed. Different nanocatalysts with Cu contents were characterized by X-ray diffraction, nitrogen porosimetry, scanning electron microscopy, and transmission electron microscopy. The TiO2 and Cu metallic nanoparticles were synthesized with copper loading up to one (Cu\/Ti atomic ratio). Synthesized catalysts exhibited pore sizes in the mesoporous range and high surface areas above 150 m2\/g. The particle size for TiO2 presented a homogeneous distribution of approximately 8 nm, moreover, Cu nanoparticles varied from 12 to &gt;100 nm depending on the metal loading. The nanostructured materials were successfully tested in the conversion of trans-ferulic acid into vanillin under sustainable conditions, achieving the best performance for 0.3 Cu\/Ti atomic ratio (70% vanillin yield).<\/jats:p>","DOI":"10.3390\/molecules24213985","type":"journal-article","created":{"date-parts":[[2019,11,4]],"date-time":"2019-11-04T10:49:07Z","timestamp":1572864547000},"page":"3985","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":13,"title":["One-Pot Cu\/TiO2 Nanoparticles Synthesis for Trans-Ferulic Acid Conversion into Vanillin"],"prefix":"10.3390","volume":"24","author":[{"given":"Paulette","family":"G\u00f3mez-L\u00f3pez","sequence":"first","affiliation":[{"name":"Departamento de Qu\u00edmica Org\u00e1nica, Universidad de Cordoba, Campus de Rabanales, Edificio Marie Curie (C-3), Ctra Nnal IV-A, Km 396, E14014 Cordoba, Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3912-1059","authenticated-orcid":false,"given":"Noelia","family":"L\u00e1zaro","sequence":"additional","affiliation":[{"name":"Departamento de Qu\u00edmica Org\u00e1nica, Universidad de Cordoba, Campus de Rabanales, Edificio Marie Curie (C-3), Ctra Nnal IV-A, Km 396, E14014 Cordoba, Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Clemente G.","family":"Alvarado-Beltr\u00e1n","sequence":"additional","affiliation":[{"name":"Facultad de Ingenier\u00eda Mochis, Universidad Aut\u00f3noma de Sinaloa, Fuente de Poseid\u00f3n y Prol. Angel Flores, S.N., Los Mochis Sin. 81223, Mexico"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Antonio","family":"Pineda","sequence":"additional","affiliation":[{"name":"Departamento de Qu\u00edmica Org\u00e1nica, Universidad de Cordoba, Campus de Rabanales, Edificio Marie Curie (C-3), Ctra Nnal IV-A, Km 396, E14014 Cordoba, Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8872-3400","authenticated-orcid":false,"given":"Alina M.","family":"Balu","sequence":"additional","affiliation":[{"name":"Departamento de Qu\u00edmica Org\u00e1nica, Universidad de Cordoba, Campus de Rabanales, Edificio Marie Curie (C-3), Ctra Nnal IV-A, Km 396, E14014 Cordoba, Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4190-1916","authenticated-orcid":false,"given":"Rafael","family":"Luque","sequence":"additional","affiliation":[{"name":"Departamento de Qu\u00edmica Org\u00e1nica, Universidad de Cordoba, Campus de Rabanales, Edificio Marie Curie (C-3), Ctra Nnal IV-A, Km 396, E14014 Cordoba, Spain"},{"name":"Scientific Center for Molecular Design and Synthesis of Innovative Compounds for the Medical Industry, People\u2019s Friendship University of Russia (RUDN University), Moscow 117198, Russia"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"1968","published-online":{"date-parts":[[2019,11,4]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"20400","DOI":"10.1038\/srep20400","article-title":"A microbial transformation using Bacillus subtilis B7-S to produce natural vanillin from ferulic acid","volume":"6","author":"Chen","year":"2015","journal-title":"Sci. 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