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Via a direct pyrolysis of the melamine\u2013formaldehyde resin spheres, the well\u2013distributed Fe\u2013NC spheres were obtained. The as\u2013prepared Fe\u2013NC possesses enhanced catalysis towards the redox of acetaminophen for abundant active sites and high\u2013speed charge transfer. The effect of loading Fe species on the electrochemical sensing of acetaminophen is investigated in detail. The synergistic effect of nitrogen doping along with the above\u2013mentioned properties is taken advantage of in the fabrication of electrochemical sensors for the acetaminophen determination. Based on the calibration plot, the limits of detection (LOD) were calculated to be 0.026 \u03bcM with a linear range from 0\u2013100 \u03bcM. Additionally satisfactory repeatability, stability, and selectivity are obtained.<\/jats:p>","DOI":"10.3390\/molecules28073006","type":"journal-article","created":{"date-parts":[[2023,3,28]],"date-time":"2023-03-28T04:37:15Z","timestamp":1679978235000},"page":"3006","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":23,"title":["Fe\u2013Decorated Nitrogen\u2013Doped Carbon Nanospheres as an Electrochemical Sensing Platform for the Detection of Acetaminophen"],"prefix":"10.3390","volume":"28","author":[{"given":"Xiangchuan","family":"Zhao","sequence":"first","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"},{"name":"Institute of Advanced Materials, Shandong Institutes of Industrial Technology, Jinan 250000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Liping","family":"Zhang","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0009-7046-4488","authenticated-orcid":false,"given":"Zhaoyun","family":"Chu","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qing","family":"Wang","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3939-2833","authenticated-orcid":false,"given":"Yue","family":"Cao","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jun","family":"Cao","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jiao","family":"Li","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wu","family":"Lei","sequence":"additional","affiliation":[{"name":"School of Chemistry and Chemical Engineering, Nanjing University of Science and Technology, Xiaolingwei 200th, Nanjing 210094, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Boming","family":"Zhang","sequence":"additional","affiliation":[{"name":"Institute of Advanced Materials, Shandong Institutes of Industrial Technology, Jinan 250000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Weimeng","family":"Si","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering, Shandong University of Technology, Xincunxi Road 266th, Zibo 255000, China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1968","published-online":{"date-parts":[[2023,3,28]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"113496","DOI":"10.1016\/j.jelechem.2019.113496","article-title":"Nitrogen\u2013rich porous carbon modified electrochemical sensor for the detection of acetaminophen","volume":"855","author":"Liang","year":"2019","journal-title":"J. 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