{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,8,21]],"date-time":"2026-08-21T23:38:05Z","timestamp":1787355485845,"version":"build-2736575974"},"reference-count":28,"publisher":"MDPI AG","issue":"20","license":[{"start":{"date-parts":[[2024,10,18]],"date-time":"2024-10-18T00:00:00Z","timestamp":1729209600000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100001809","name":"Natural Science Foundation of China","doi-asserted-by":"publisher","award":["52003071"],"award-info":[{"award-number":["52003071"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100001809","name":"Natural Science Foundation of China","doi-asserted-by":"publisher","award":["2022KLIB03"],"award-info":[{"award-number":["2022KLIB03"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]},{"name":"Open Project of Key Laboratory of Fire Protection Technology for Industry and Public Building, the Ministry of Emergency Management, China","award":["52003071"],"award-info":[{"award-number":["52003071"]}]},{"name":"Open Project of Key Laboratory of Fire Protection Technology for Industry and Public Building, the Ministry of Emergency Management, China","award":["2022KLIB03"],"award-info":[{"award-number":["2022KLIB03"]}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Molecules"],"abstract":"<jats:p>In order to prepare flexible thermal protection aerogel materials, using dimethyldimethoxysilane (DMDMS) and methyltrimethoxysilane (MTMS) as co-precursors, isocyanate-propyltrimethoxysilane (CFS-006) was added to the co-precursor as a coupling agent, and resorcinol and formaldehyde were added to the sol solution to prepare a phenolic silicone hybrid aerogel (FAS) by the sol\u2013gel method. The prepared FAS aerogel had no phase separation problem, the density was only 0.118 g\/cm3, the hydrophobic angle reached 155.3\u00b0, and it had certain flexibility. It could be compressed to 70% and still be restored to its original state. The FAS aerogel also had a low thermal conductivity of 0.0318 W\/(m\u00b7K) and good high temperature insulation. The introduction of phenolic groups improved thermal stability; Tmax increased to 643.7 \u00b0C, and the residual carbon rate was 24.5%. This work has positive significance for the future combination of aerogels and textiles in the preparation of firefighting protective clothing.<\/jats:p>","DOI":"10.3390\/molecules29204942","type":"journal-article","created":{"date-parts":[[2024,10,21]],"date-time":"2024-10-21T09:58:24Z","timestamp":1729504704000},"page":"4942","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":11,"title":["Preparation and Properties of Flexible Phenolic Silicone Hybrid Aerogels for Thermal Insulation"],"prefix":"10.3390","volume":"29","author":[{"given":"Danni","family":"Ye","sequence":"first","affiliation":[{"name":"School of Textile Science and Engineering, Tiangong University, Tianjin 300387, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hongli","family":"Lv","sequence":"additional","affiliation":[{"name":"SWOTO (Beijing) Protection Technology Co., Ltd., Beijing 100041, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3527-6467","authenticated-orcid":false,"given":"Zhenrong","family":"Zheng","sequence":"additional","affiliation":[{"name":"School of Textile Science and Engineering, Tiangong University, Tianjin 300387, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lijuan","family":"Luo","sequence":"additional","affiliation":[{"name":"Aerospace Research Institute of Materials and Processing Technology, Beijing 100076, China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1968","published-online":{"date-parts":[[2024,10,18]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"55","DOI":"10.1080\/00405167.2016.1179477","article-title":"Aerogels for thermal insulation in high-performance textiles","volume":"48","author":"Jamshaid","year":"2016","journal-title":"Text. 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