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fiber-reinforced SiC composites were investigated in this work. First, \u03b1-Al2O3 nanoparticles were added to the carbon fiber bundles using a slurry impregnation method, and then the Cf\/SiC composite with an \u03b1-Al2O3 nanoparticle filler (Cf\/SiC-Al2O3) was fabricated using a precursor infiltration and pyrolysis method. The microstructure of the Cf\/SiC-Al2O3 composite showed chemical compatibility between the \u03b1-Al2O3 and the pyrolysis SiC. The Cf\/SiC-Al2O3 composite with a low porosity of ~6.67% achieved a good flexural strength of 629.3 MPa and a good fracture toughness of 25.2 MPa\u00b7m1\/2. The interlaminar shear strength of the Cf\/SiC-Al2O3 composite was 11.7 MPa. The SiC-Al2O3 matrix also presented a considerable Young\u2019s modulus of 138.2 \u00b1 8.66 GPa and hardness of 10.3 \u00b1 1.03 GPa. Further analysis indicated that the good mechanical properties with the addition of an \u03b1-Al2O3 filler were not only related to the dense matrix and the improvement of the mechanical properties of the matrix. They also originated from the thermal residual compressive stress in the SiC matrix close to the \u03b1-Al2O3 nanoparticles caused by the thermal expansion mismatch, which could reflect and close the cracks in the matrix. The findings of this study provide more methods for designing new composites exhibiting a good performance.<\/jats:p>","DOI":"10.3390\/nano12193406","type":"journal-article","created":{"date-parts":[[2022,9,28]],"date-time":"2022-09-28T22:53:19Z","timestamp":1664405599000},"page":"3406","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":10,"title":["Microstructure and Mechanical Properties of Unidirectional, Laminated Cf\/SiC Composites with \u03b1-Al2O3 Nanoparticles as Filler"],"prefix":"10.3390","volume":"12","author":[{"given":"Lixia","family":"Yang","sequence":"first","affiliation":[{"name":"College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, 29 Yudao St., Nanjing 210016, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fei","family":"Wang","sequence":"additional","affiliation":[{"name":"College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, 29 Yudao St., Nanjing 210016, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jiahao","family":"Liao","sequence":"additional","affiliation":[{"name":"College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, 29 Yudao St., Nanjing 210016, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhaofeng","family":"Chen","sequence":"additional","affiliation":[{"name":"College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, 29 Yudao St., Nanjing 210016, China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zongde","family":"Kou","sequence":"additional","affiliation":[{"name":"Herbert Gleiter Institute of Nanoscience, School of Materials Science and Engineering, Nanjing University of Science and Technology, Nanjing 210094, China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1968","published-online":{"date-parts":[[2022,9,28]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","first-page":"155","DOI":"10.1016\/S0266-3538(03)00230-6","article-title":"Design, preparation and properties of non-oxide CMCs for application in engines and nuclear reactors: An overview","volume":"64","author":"Naslain","year":"2004","journal-title":"Compos. 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