{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,12,6]],"date-time":"2025-12-06T17:20:42Z","timestamp":1765041642671,"version":"build-2065373602"},"reference-count":54,"publisher":"MDPI AG","issue":"3","license":[{"start":{"date-parts":[[2025,2,27]],"date-time":"2025-02-27T00:00:00Z","timestamp":1740614400000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"name":"NGS\u2014New Generation Storage","award":["02\/C05-i01.01\/2022.PC644936001-00000045","UIDB\/50022\/2020"],"award-info":[{"award-number":["02\/C05-i01.01\/2022.PC644936001-00000045","UIDB\/50022\/2020"]}]},{"name":"the Recovery and Resilience Plan and by European Funds Next Generation EU","award":["02\/C05-i01.01\/2022.PC644936001-00000045","UIDB\/50022\/2020"],"award-info":[{"award-number":["02\/C05-i01.01\/2022.PC644936001-00000045","UIDB\/50022\/2020"]}]},{"name":"Funda\u00e7\u00e3o para a Ci\u00eancia e a Tecnologia (FCT)","award":["02\/C05-i01.01\/2022.PC644936001-00000045","UIDB\/50022\/2020"],"award-info":[{"award-number":["02\/C05-i01.01\/2022.PC644936001-00000045","UIDB\/50022\/2020"]}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Batteries"],"abstract":"<jats:p>This study explores the preparation of lithium iron phosphate (LFP) electrodes for lithium-ion batteries (LIBs), focusing on electrode loadings, dispersion techniques, and drying methods. Using a three-roll mill for LFP slurry dispersion, good electrochemical properties were achieved with loadings of 5\u20138 mg\u00b7cm\u22122 (0.8\u20131.2 mAh\u00b7cm\u22122 areal capacity). Adding polyvinylidene fluoride (PVDF) during the final milling stage reduced performance due to premature solidification in-between rolls. Vacuum-free drying improved ionic conductivity, stability against lithium metal, and discharge capacity, whereas vacuum-dried samples exhibited higher initial resistance and lower capacity retention. These findings highlight critical parameters for enhancing LFP electrode performance, paving the way for high-performance, and sustainable energy-storage solutions.<\/jats:p>","DOI":"10.3390\/batteries11030093","type":"journal-article","created":{"date-parts":[[2025,2,28]],"date-time":"2025-02-28T10:46:46Z","timestamp":1740739606000},"page":"93","update-policy":"https:\/\/doi.org\/10.3390\/mdpi_crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["A Comprehensive Study of LFP-Based Positive Electrodes: Process Parameters\u2019 Influence on the Electrochemical Properties"],"prefix":"10.3390","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-5252-4760","authenticated-orcid":false,"given":"Beatriz","family":"Arouca Maia","sequence":"first","affiliation":[{"name":"Materials and Composite Structures Unit (UMEC), Institute of Science and Innovation in Mechanical and Industrial Engineering (INEGI), 4200-465 Porto, Portugal"},{"name":"Faculty of Engineering, University of Porto, 4200-465 Porto, Portugal"},{"name":"Materials for Energy Research Laboratory (MatER), University of Porto, 4200-465 Porto, Portugal"},{"name":"Associated Laboratory of Energy, Transports and Aerospace (LAETA), 4200-265 Porto, Portugal"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7924-589X","authenticated-orcid":false,"given":"Nat\u00e1lia","family":"Magalh\u00e3es","sequence":"additional","affiliation":[{"name":"Materials and Composite Structures Unit (UMEC), Institute of Science and Innovation in Mechanical and Industrial Engineering (INEGI), 4200-465 Porto, Portugal"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8452-1783","authenticated-orcid":false,"given":"Eunice","family":"Cunha","sequence":"additional","affiliation":[{"name":"Materials and Composite Structures Unit (UMEC), Institute of Science and Innovation in Mechanical and Industrial Engineering (INEGI), 4200-465 Porto, Portugal"}]},{"given":"Nuno","family":"Correia","sequence":"additional","affiliation":[{"name":"Materials and Composite Structures Unit (UMEC), Institute of Science and Innovation in Mechanical and Industrial Engineering (INEGI), 4200-465 Porto, Portugal"},{"name":"Associated Laboratory of Energy, Transports and Aerospace (LAETA), 4200-265 Porto, Portugal"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4577-2154","authenticated-orcid":false,"given":"Maria Helena","family":"Braga","sequence":"additional","affiliation":[{"name":"Faculty of Engineering, University of Porto, 4200-465 Porto, Portugal"},{"name":"Materials for Energy Research Laboratory (MatER), University of Porto, 4200-465 Porto, Portugal"},{"name":"Associated Laboratory of Energy, Transports and Aerospace (LAETA), 4200-265 Porto, Portugal"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1050-1808","authenticated-orcid":false,"given":"Raquel M.","family":"Santos","sequence":"additional","affiliation":[{"name":"Materials and Composite Structures Unit (UMEC), Institute of Science and Innovation in Mechanical and Industrial Engineering (INEGI), 4200-465 Porto, Portugal"},{"name":"Associated Laboratory of Energy, Transports and Aerospace (LAETA), 4200-265 Porto, Portugal"}]}],"member":"1968","published-online":{"date-parts":[[2025,2,27]]},"reference":[{"key":"ref_1","doi-asserted-by":"crossref","unstructured":"Guerreiro, A.N., Maia, B.A., Khalifa, H., Baptista, M.C., and Braga, M.H. 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