{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,12,6]],"date-time":"2025-12-06T04:58:35Z","timestamp":1764997115133},"reference-count":0,"publisher":"Oxford University Press (OUP)","issue":"3","license":[{"start":{"date-parts":[[2017,5,1]],"date-time":"2017-05-01T00:00:00Z","timestamp":1493596800000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/academic.oup.com\/journals\/pages\/open_access\/funder_policies\/chorus\/standard_publication_model"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2017,5,1]]},"abstract":"<jats:title>Abstract<\/jats:title>\n               <jats:p>An economical, rapid, and sensitive multiresidue method using liquid\u2013liquid extraction (LLE) coupledwith dispersive SPE (dSPE) cleanup was developed for the quantitative determination of 34 multiclass multiresidue (MCMR) pesticides (14 organochlorines, eight organophosphates, 10 synthetic pyrethroids, and two herbicides) in nonalcoholic carbonated beverages (cola, orange, lemon-lime, and citra) using GC with tandem MS. The procedure mainly involved LLE by dichloromethane and dSPE cleanup in the presence of magnesium sulfate, primary secondary amine, and C18. The RSD of the developed method was found to be less than 14%. The LOD andLOQ values for all the analyzed pesticides were found in the ranges of 0.001\u20130.027 \u03bcg\/L and 0.004\u20130.088 \u03bcg\/L, respectively. The LOQ levels of the pesticides analyzed were found to be well below the recommended limit by the European Union (0.1 \u03bcg\/L in water). The mean recoveries of pesticides indifferent nonalcoholic carbonated beverages (cola, orange, lemon-lime, and citra) were found to be in the range of 79\u2013111%, with RSDs less than 11%. The validation data prove that the method can be acceptable to regulatory agencies for the routine analysis of MCMR pesticides in nonalcoholic carbonated beverages.<\/jats:p>","DOI":"10.5740\/jaoacint.17-0064","type":"journal-article","created":{"date-parts":[[2017,3,17]],"date-time":"2017-03-17T11:05:57Z","timestamp":1489748757000},"page":"624-630","source":"Crossref","is-referenced-by-count":7,"title":["A Rapid Method for the Quantitative Determination of 34 Pesticides in Nonalcoholic Carbonated Beverages Using Liquid\u2013Liquid Extraction Coupled to Dispersive Solid-Phase Cleanup Followed by Gas Chromatography with Tandem Mass Spectrometry"],"prefix":"10.1093","volume":"100","author":[{"given":"Satyajeet","family":"Rai","sequence":"first","affiliation":[{"name":"Council of Scientific and Industrial Research\u2013Indian Institute of Toxicology Research, Regulatory Toxicology Group, Pesticide Toxicology Laboratory, Vish Vigyan Bhavan MG Marg, Lucknow 226 001, Uttar Pradesh, India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Madhuri Devi","family":"Gullapalli","sequence":"additional","affiliation":[{"name":"Council of Scientific and Industrial Research\u2013Indian Institute of Chemical Technology, Analytical Chemistry and Mass Spectrometry Division, Chromatography Unit, Tarnaka, Uppal Rd, Hyderabad 500 007, Telangana, India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Anshuman","family":"Srivastava","sequence":"additional","affiliation":[{"name":"Council of Scientific and Industrial Research\u2013Indian Institute of Toxicology Research, Regulatory Toxicology Group, Pesticide Toxicology Laboratory, Vish Vigyan Bhavan MG Marg, Lucknow 226 001, Uttar Pradesh, India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Hussain","family":"Shaik","sequence":"additional","affiliation":[{"name":"Council of Scientific and Industrial Research\u2013Indian Institute of Chemical Technology, Analytical Chemistry and Mass Spectrometry Division, Chromatography Unit, Tarnaka, Uppal Rd, Hyderabad 500 007, Telangana, India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Mohammed Haris","family":"Siddiqui","sequence":"additional","affiliation":[{"name":"Integral University, Department of Bioengineering, Lucknow 226 026, Uttar Pradesh, India"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Mohana Krishna Reddy","family":"Mudiam","sequence":"additional","affiliation":[{"name":"Council of Scientific and Industrial Research\u2013Indian Institute of Chemical Technology, Analytical Chemistry and Mass Spectrometry Division, Chromatography Unit, Tarnaka, Uppal Rd, Hyderabad 500 007, Telangana, India"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"286","published-online":{"date-parts":[[2019,11,22]]},"container-title":["Journal of AOAC INTERNATIONAL"],"original-title":[],"language":"en","link":[{"URL":"http:\/\/academic.oup.com\/jaoac\/article-pdf\/100\/3\/624\/32427925\/jaoac0624.pdf","content-type":"application\/pdf","content-version":"vor","intended-application":"syndication"},{"URL":"http:\/\/academic.oup.com\/jaoac\/article-pdf\/100\/3\/624\/32427925\/jaoac0624.pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2020,3,19]],"date-time":"2020-03-19T18:16:57Z","timestamp":1584641817000},"score":1,"resource":{"primary":{"URL":"https:\/\/academic.oup.com\/jaoac\/article\/100\/3\/624-630\/5654181"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2017,5,1]]},"references-count":0,"journal-issue":{"issue":"3","published-online":{"date-parts":[[2019,11,22]]},"published-print":{"date-parts":[[2017,5,1]]}},"URL":"https:\/\/doi.org\/10.5740\/jaoacint.17-0064","relation":{},"ISSN":["1060-3271","1944-7922"],"issn-type":[{"value":"1060-3271","type":"print"},{"value":"1944-7922","type":"electronic"}],"subject":[],"published-other":{"date-parts":[[2017,5,1]]},"published":{"date-parts":[[2017,5,1]]}}}